{"product_id":"thermal-analysis-of-polymers-isbn-9780471769170","title":"Thermal Analysis of Polymers","description":"\u003cul\u003e \u003cli\u003ePresents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background.\u003c\/li\u003e \u003cli\u003eUseful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications\u003c\/li\u003e \u003cli\u003eTopics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC\/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation.\u003c\/li\u003e \u003cli\u003eWritten by experts in the various areas of thermal analysis\u003c\/li\u003e \u003cli\u003eRelevant and detailed experiments and examples follow each chapter.\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003ePreface ix\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1 Introduction 1\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eJoseph D. Menczel, R. Bruce Prime and Patrick K. Gallagher\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2 Differential Scanning Calorimetry (DSC) 7\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eJoseph D. Menczel, Lawrence Judovits, R. Bruce Prime, Harvey E. Bair, Mike Reading, and Steven Swier\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e2.1. Introduction 7\u003c\/p\u003e \u003cp\u003e2.2. Elements of Thermodynamics in DSC 9\u003c\/p\u003e \u003cp\u003e2.3. The Basics of Differential Scanning Calorimetry 18\u003c\/p\u003e \u003cp\u003e2.4. Purity Determination of Low-Molecular-Mass Compounds by DSC 37\u003c\/p\u003e \u003cp\u003e2.5. Calibration of Differential Scanning Calorimeters 41\u003c\/p\u003e \u003cp\u003e2.6. Measurement of Heat Capacity 52\u003c\/p\u003e \u003cp\u003e2.7. Phase Transitions in Amorphous and Crystalline Polymers 58\u003c\/p\u003e \u003cp\u003e2.8. Fibers 115\u003c\/p\u003e \u003cp\u003e2.9. Films 123\u003c\/p\u003e \u003cp\u003e2.10. Thermosets 130\u003c\/p\u003e \u003cp\u003e2.11. Differential Photocalorimetry (DPC) 154\u003c\/p\u003e \u003cp\u003e2.12. Fast-Scan DSC 162\u003c\/p\u003e \u003cp\u003e2.13. Modulated Temperature Differential Scanning Calorimetry (MTDSC) 168\u003c\/p\u003e \u003cp\u003e2.14. How to Perform DSC Measurements 208\u003c\/p\u003e \u003cp\u003e2.15. Instrumentation 217\u003c\/p\u003e \u003cp\u003eAppendix 225\u003c\/p\u003e \u003cp\u003eAbbreviations 225\u003c\/p\u003e \u003cp\u003eReferences 229\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3 Thermogravimetric Analysis (TGA) 241\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eR. Bruce Prime, Harvey E. Bair, Sergey Vyazovkin, Patrick K. Gallagher, and Alan Riga\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e3.1. Introduction 241\u003c\/p\u003e \u003cp\u003e3.2. Background Principles and Measurement Modes 242\u003c\/p\u003e \u003cp\u003e3.3. Calibration and Reference Materials 251\u003c\/p\u003e \u003cp\u003e3.4. Measurements and Analyses 256\u003c\/p\u003e \u003cp\u003e3.5. Kinetics 277\u003c\/p\u003e \u003cp\u003e3.6. Selected Applications 295\u003c\/p\u003e \u003cp\u003e3.7. Instrumentation 308\u003c\/p\u003e \u003cp\u003eAppendix 311\u003c\/p\u003e \u003cp\u003eAbbreviations 312\u003c\/p\u003e \u003cp\u003eReferences 314\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4 Thermomechanical Analysis (TMA) and Thermodilatometry (TD) 319\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eHarvey E. Bair, Ali E. Akinay, Joseph D. Menczel, R. Bruce Prime, and Michael Jaffe\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e4.1. Introduction 319\u003c\/p\u003e \u003cp\u003e4.2. Principles and Theory 320\u003c\/p\u003e \u003cp\u003e4.3. Instrumental 326\u003c\/p\u003e \u003cp\u003e4.4. Calibration 332\u003c\/p\u003e \u003cp\u003e4.5. How to Perform a TMA Experiment 335\u003c\/p\u003e \u003cp\u003e4.6. Key Applications 340\u003c\/p\u003e \u003cp\u003e4.7. Selected Industrial Applications (with Details of Experimental Conditions) 363\u003c\/p\u003e \u003cp\u003eAppendix 378\u003c\/p\u003e \u003cp\u003eAbbreviations 380\u003c\/p\u003e \u003cp\u003eReferences 381\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5 Dynamic Mechanical Analysis (DMA) 387\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eRichard P. Chartoff, Joseph D. Menczel, and Steven H. Dillman\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e5.1. Introduction 387\u003c\/p\u003e \u003cp\u003e5.2. Characterization of Viscoelastic Behavior 394\u003c\/p\u003e \u003cp\u003e5.3. The Relationship between Time, Temperature, and Frequency 401\u003c\/p\u003e \u003cp\u003e5.4. Applications of Dynamic Mechanical Analysis 410\u003c\/p\u003e \u003cp\u003e5.5. Examples of DMA Characterization for Thermoplastics 424\u003c\/p\u003e \u003cp\u003e5.6. Characteristics of Fibers and Thin Films 432\u003c\/p\u003e \u003cp\u003e5.7. DMA Characterization of Crosslinked Polymers 438\u003c\/p\u003e \u003cp\u003e5.8. Practical Aspects of Conducting DMA Experiments 456\u003c\/p\u003e \u003cp\u003e5.9. Commercial DMA Instrumentation 477\u003c\/p\u003e \u003cp\u003eAppendix 488\u003c\/p\u003e \u003cp\u003eAbbreviations 489\u003c\/p\u003e \u003cp\u003eReferences 491\u003c\/p\u003e \u003cp\u003e\u003cb\u003e6 Dielectric Analysis (DEA) 497\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eAglaia Vassilikou-Dova and Ioannis M. Kalogeras\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e6.1. Introduction 497\u003c\/p\u003e \u003cp\u003e6.2. Theory and Background of Dielectric Analysis 502\u003c\/p\u003e \u003cp\u003e6.3. Dielectric Techniques 520\u003c\/p\u003e \u003cp\u003e6.4. Performing Dielectric Experiments 528\u003c\/p\u003e \u003cp\u003e6.5. Typical Measurements on Poly(Methyl Methacrylate) (PMMA) 538\u003c\/p\u003e \u003cp\u003e6.6. Dielectric Analysis of Thermoplastics 553\u003c\/p\u003e \u003cp\u003e6.7. Dielectric Analysis of Thermosets 576\u003c\/p\u003e \u003cp\u003e6.8. Instrumentation 592\u003c\/p\u003e \u003cp\u003eAppendix 599\u003c\/p\u003e \u003cp\u003eAbbreviations 599\u003c\/p\u003e \u003cp\u003eReferences 603\u003c\/p\u003e \u003cp\u003e\u003cb\u003e7 Micro- And Nanoscale Local Thermal Analysis 615\u003c\/b\u003e\u003cbr\u003e \u003ci\u003eValeriy V Gorbunov, David Grandy, Mike Reading, and Vladimir V. Tsukruk\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e7.1. Introduction 615\u003c\/p\u003e \u003cp\u003e7.2. The Atomic Force Microscope 616\u003c\/p\u003e \u003cp\u003e7.3. Scanning Thermal Microscopy 618\u003c\/p\u003e \u003cp\u003e7.4. Thermal Probe Design and Spatial Resolution 620\u003c\/p\u003e \u003cp\u003e7.5. Measuring Thermal Conductivity and Thermal Force-Distance Curves 624\u003c\/p\u003e \u003cp\u003e7.6. Local Thermal Analysis 628\u003c\/p\u003e \u003cp\u003e7.7. Performing a Micro\/Nanoscale Thermal Analysis Experiment 633\u003c\/p\u003e \u003cp\u003e7.8. Examples of Micro\/Nanoscale Thermal Analysis Applications 637\u003c\/p\u003e \u003cp\u003e7.9. Overview of Local Thermal Analysis 644\u003c\/p\u003e \u003cp\u003eAbbreviations 647\u003c\/p\u003e \u003cp\u003eReferences 648\u003c\/p\u003e \u003cp\u003eIndex 651\u003c\/p\u003e  \"I have read it with great pleasure and it is my honor to provide this short review. Let me congratulate the editors on the concept of this book. They managed to tune the balance between basic principles and practical information finely . . .In conclusion I think that this book is very useful for students, PhDs, and researchers who are dealing or intended to deal with thermal analysis of polymers.\" (J Therm Anal Calorim, 2010)  \u003cp\u003e \u003c\/p\u003e  \u003cp\u003eJoseph D. Menczel, PhD, a recognized expert in thermal analysis of polymers with some thirty years of industrial and academic experience, is Assistant Technical Director at Alcon Laboratories. He has researched more than 120 polymeric systems in which he studied calibration of DSCs, glass transition, nucleation, crystallization, melting, stability, mechanical and micro-mechanical properties of polymers, and polymer-water interactions. Dr. Menczel holds six patents and is the author of seventy scholarly papers. He is the author of two chapters in the bookThermal Characterization of Polymeric Materials. In conducting DSC experiments, Dr. Menczel found a crystal\/amorphous interface in semicrystalline polymers, which later became known as the rigid amorphous phase. He is also credited with developing the temperature calibration of DSCs for cooling experiments.\u003c\/p\u003e \u003cp\u003eR. Bruce Prime, PhD, is a consultant to industry and government and a recognized authority on the cure and properties of cross-linked polymer systems. During his thirty-year career with IBM, he led teams responsible for developing and implementing polymer applications for printer and information storage technologies. He holds four patents and is the author of more than fifty technical papers and the chapter on thermosets in Thermal Characterization of Polymeric Materials. Dr. Prime is a Fellow of SPE and NATAS and was the 1989 recipient of the Mettler-Toledo Award in Thermal Analysis. He maintains the Web site www.primethermosets.com.\u003c\/p\u003e  \u003cp\u003eLearn how to take full advantage of a broad range of thermal analysis techniques\u003c\/p\u003e \u003cp\u003eThermal Analysis of Polymers: Fundamentals and Applications emphasizes the practical uses of thermal analysis, enabling readers to take full advantage of its capabilities as a polymer characterization tool in their laboratories. The book offers essential theoretical background; however, it focuses on how to perform a broad range of thermal analysis measurements and tests, with detailed coverage of methods, applications, instrumentation, and calibration. Moreover, it helps readers correctly interpret their results.\u003c\/p\u003e \u003cp\u003eThis book features a team of authors whose expertise spans all the thermal analysis techniques and applications covered in the book. Their advice is based not only on thorough knowledge of the literature, but also their own hands-on experience working in the lab. Among the topics covered are:\u003c\/p\u003e \u003cul\u003e \u003cli\u003e \u003cp\u003eDifferential scanning calorimetry\u003c\/p\u003e \u003c\/li\u003e \u003cli\u003e \u003cp\u003eThermogravimetric analysis\u003c\/p\u003e \u003c\/li\u003e \u003cli\u003e \u003cp\u003eThermomechanical analysis and thermodilatometry\u003c\/p\u003e \u003c\/li\u003e \u003cli\u003e \u003cp\u003eDynamic mechanical analysis\u003c\/p\u003e \u003c\/li\u003e \u003cli\u003e \u003cp\u003eDielectric analysis\u003c\/p\u003e \u003c\/li\u003e \u003cli\u003e \u003cp\u003eMicro- and nano-scale local thermal analysis\u003c\/p\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003eEach chapter guides readers through the applications of thermal analysis for polymer char-acterization, with detailed examples that show how to perform each step. References guide readers to the primary literature for further investigation into each topic.\u003c\/p\u003e \u003cp\u003eFollowing this book's step-by-step guidance, chemists and engineers new to thermal analysis techniques, whether in industry, government, or academia, can quickly learn to use them to generate high-quality results. For more experienced researchers, the book enables them to expand their repertoire to include a broader range of sophisticated techniques and applications.\u003c\/p\u003e","brand":"Wiley","offers":[{"title":"Default Title","offer_id":47990382756069,"sku":"NP9780471769170","price":216.95,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9780471769170.jpg?v=1761787603","url":"https:\/\/k12savings.com\/products\/thermal-analysis-of-polymers-isbn-9780471769170","provider":"K12savings","version":"1.0","type":"link"}