{"product_id":"the-systematic-identification-of-organic-compounds-isbn-9781119799665","title":"The Systematic Identification of Organic Compounds","description":"\u003cb\u003eThe Systematic Identification of Organic Compounds\u003c\/b\u003e \u003cp\u003e\u003cb\u003eA comprehensive introduction to the identification of unknown organic compounds\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eIdentifying unknown compounds is one of the most important parts of the study of chemistry. From basic characteristics such as melting and\/or boiling point to more complex data generated through cutting-edge techniques, the range of possible methods for identifying unknown organic compounds is substantial. The utility of a research reference which compiles known techniques and characteristics of possible compounds is clear.\u003c\/p\u003e \u003cp\u003e\u003ci\u003eThe Systematic Identification of Organic Compounds \u003c\/i\u003eprovides such a reference, designed to teach a hands-on approach in the chemistry lab. It takes readers step-by-step through the process of identifying an unknown compound and elucidating its structure from infrared, nuclear magnetic resonance, and mass spectra in addition to solubility characteristics, melting point, boiling point, and classification tests. The result is an essential overview for advanced chemistry students looking to understand this exciting area of laboratory work.\u003c\/p\u003e \u003cp\u003eReaders of the ninth edition of \u003ci\u003eThe Systematic Identification of Organic Compounds \u003c\/i\u003ewill also find:\u003c\/p\u003e \u003cul\u003e \u003cli\u003eA detailed chapter on safety, personal protection equipment, chemical storage, safety data sheets, and other safety concerns\u003c\/li\u003e \u003cli\u003eNew NMR, IR, and mass spectra with detailed explanations on interpretation\u003c\/li\u003e \u003cli\u003eQuestions at the end of each chapter designed to facilitate and reinforce progression, keyed to a companion website for instructors\u003c\/li\u003e \u003cli\u003eTables of known compounds including data relevant for identification\u003c\/li\u003e \u003cli\u003eCompanion website with structural problems from experimental data for students to practice how to reason and solve\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003ci\u003eThe Systematic Identification of Organic Compounds \u003c\/i\u003eis a useful reference for advanced undergraduates and graduate students studying organic chemistry, organic spectroscopy, and related subjects.\u003c\/p\u003e \u003cp\u003ePreface ix\u003c\/p\u003e \u003cp\u003eAbout the Companion Website xi\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 1 Introduction 1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e1.1 Systematic Identification of Organic Compounds: The Need for Organic Qualitative Analysis 1\u003c\/p\u003e \u003cp\u003e1.2 Suggestions to Students and Instructors 3\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 2 Laboratory Safety 7\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e2.1 Working Safely in the Laboratory 7\u003c\/p\u003e \u003cp\u003e2.2 Training 10\u003c\/p\u003e \u003cp\u003e2.3 Personal Protection Equipment 10\u003c\/p\u003e \u003cp\u003e2.4 Safety Data Sheets 11\u003c\/p\u003e \u003cp\u003e2.5 Storage of Chemicals 12\u003c\/p\u003e \u003cp\u003e2.6 Disposal of Chemicals 13\u003c\/p\u003e \u003cp\u003e2.7 Safely Using Equipment in the Laboratory 13\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 3 Identification of Unknowns 15\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e3.1 Discussion of Report Form 15\u003c\/p\u003e \u003cp\u003e3.2 Preliminary Examination 22\u003c\/p\u003e \u003cp\u003e3.3 Physical Properties 22\u003c\/p\u003e \u003cp\u003e3.4 Molecular Weight Determination 22\u003c\/p\u003e \u003cp\u003e3.5 Molecular Formula Determination 23\u003c\/p\u003e \u003cp\u003e3.6 Solubility Tests 23\u003c\/p\u003e \u003cp\u003e3.7 Infrared, Nuclear Magnetic Resonance, and Mass Spectra Analyses 24\u003c\/p\u003e \u003cp\u003e3.8 Classification Tests 24\u003c\/p\u003e \u003cp\u003e3.9 Preparation of a Satisfactory Derivative 25\u003c\/p\u003e \u003cp\u003e3.10 Mixtures 26\u003c\/p\u003e \u003cp\u003e3.11 Report Forms 26\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 4 Preliminary Examination, Physical Properties, and Elemental Analysis 31\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e4.1 Preliminary Examination 32\u003c\/p\u003e \u003cp\u003e4.2 Determination of Physical Properties 34\u003c\/p\u003e \u003cp\u003e4.3 Optical Rotation 53\u003c\/p\u003e \u003cp\u003e4.4 Recrystallization 58\u003c\/p\u003e \u003cp\u003e4.5 Qualitative Elemental Analysis 61\u003c\/p\u003e \u003cp\u003e4.6 Quantitative Elemental Analysis 69\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 5 Classification of Organic Compounds by Solubility 75\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e5.1 Solubility in Water, Aqueous Acids and Bases, and Ether 76\u003c\/p\u003e \u003cp\u003e5.2 Solubility in Organic Solvents 95\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 6 Separation of Mixtures 99\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e6.1 Preliminary Examinations of Mixtures 100\u003c\/p\u003e \u003cp\u003e6.2 Distillation and Sublimation 101\u003c\/p\u003e \u003cp\u003e6.3 Extractions: Separations Based Upon\u003c\/p\u003e \u003cp\u003e6.4 Chromatography 119\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 7 Nuclear Magnetic Resonance Spectrometry 145\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e7.1 Theory of Nuclear Magnetic Resonance 145\u003c\/p\u003e \u003cp\u003e7.2 Preparation of the Sample 149\u003c\/p\u003e \u003cp\u003e7.3 Proton Spectra 151\u003c\/p\u003e \u003cp\u003e7.4 13C Spectra 165\u003c\/p\u003e \u003cp\u003e7.5 DEPT 179\u003c\/p\u003e \u003cp\u003e7.6 COSY 188\u003c\/p\u003e \u003cp\u003e7.7 HSQC 190\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 8 Infrared Spectrometry 227\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e8.1 Theory of Infrared Spectrometry 227\u003c\/p\u003e \u003cp\u003e8.2 Preparation of the Sample 230\u003c\/p\u003e \u003cp\u003e8.3 Functional Group Identification 234\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 9 Mass Spectrometry 269\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e9.1 Theory of Mass Spectrometry 269\u003c\/p\u003e \u003cp\u003e9.2 Cleavage Reactions 271\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 10 Chemical Tests for Functional Groups 293\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e10.1 Acid Anhydrides 296\u003c\/p\u003e \u003cp\u003e10.2 Acyl Halides 306\u003c\/p\u003e \u003cp\u003e10.3 Alcohols 307\u003c\/p\u003e \u003cp\u003e10.4 Aldehydes 323\u003c\/p\u003e \u003cp\u003e10.5 Amides 332\u003c\/p\u003e \u003cp\u003e10.6 Amines and Amine Salts 334\u003c\/p\u003e \u003cp\u003e10.7 Amino Acids 349\u003c\/p\u003e \u003cp\u003e10.8 Carbohydrates 351\u003c\/p\u003e \u003cp\u003e10.9 Carboxylic Acids 359\u003c\/p\u003e \u003cp\u003e10.10 Esters 360\u003c\/p\u003e \u003cp\u003e10.11 Ethers 361\u003c\/p\u003e \u003cp\u003e10.12 Halides 365\u003c\/p\u003e \u003cp\u003e10.13 Hydrocarbons--Alkanes 371\u003c\/p\u003e \u003cp\u003e10.14 Hydrocarbons--Alkenes 371\u003c\/p\u003e \u003cp\u003e10.15 Hydrocarbons--Alkynes 378\u003c\/p\u003e \u003cp\u003e10.16 Hydrocarbons--Aromatic 379\u003c\/p\u003e \u003cp\u003e10.17 Ketones 384\u003c\/p\u003e \u003cp\u003e10.18 Nitriles 386\u003c\/p\u003e \u003cp\u003e10.19 Nitro Compounds 386\u003c\/p\u003e \u003cp\u003e10.20 Phenols 389\u003c\/p\u003e \u003cp\u003e10.21 Sulfonamides, Sulfonic Acids, Sulfonyl Chlorides 393\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 11 The Preparation of Derivatives 397\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e11.1 Carboxylic Acids, Acid Anhydrides, Acid Halides 397\u003c\/p\u003e \u003cp\u003e11.2 Alcohols 409\u003c\/p\u003e \u003cp\u003e11.3 Aldehydes And Ketones 414\u003c\/p\u003e \u003cp\u003e11.4 Amides 420\u003c\/p\u003e \u003cp\u003e11.5 Amines 424\u003c\/p\u003e \u003cp\u003e11.6 Amino Acids 432\u003c\/p\u003e \u003cp\u003e11.7 Carbohydrates 437\u003c\/p\u003e \u003cp\u003e11.8 Esters 440\u003c\/p\u003e \u003cp\u003e11.9 Ethers--Aliphatic 450\u003c\/p\u003e \u003cp\u003e11.10 Ethers--Aromatic 451\u003c\/p\u003e \u003cp\u003e11.11 Halides--Alkyl 454\u003c\/p\u003e \u003cp\u003e11.12 Halides--Aromatic 457\u003c\/p\u003e \u003cp\u003e11.13 Hydrocarbons--Aromatic 460\u003c\/p\u003e \u003cp\u003e11.14 Nitriles 462\u003c\/p\u003e \u003cp\u003e11.15 Nitro Compounds 467\u003c\/p\u003e \u003cp\u003e11.16 Phenols 468\u003c\/p\u003e \u003cp\u003e11.17 Sulfonic Acids, Sulfonyl Chlorides, Sulfonamides 472\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 12 Chemical Literature 479\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e12.1 Handbooks 480\u003c\/p\u003e \u003cp\u003e12.2 Compendia 480\u003c\/p\u003e \u003cp\u003e12.3 Spectral Collections 481\u003c\/p\u003e \u003cp\u003e12.4 Journals 482\u003c\/p\u003e \u003cp\u003e12.5 Abstracts and Indexes 483\u003c\/p\u003e \u003cp\u003e12.6 Monographs 486\u003c\/p\u003e \u003cp\u003eAppendix I Handy Tables for the Organic Laboratory 487\u003c\/p\u003e \u003cp\u003eAPPENDIX II Table of Derivatives 493\u003c\/p\u003e \u003cp\u003eAppendix III Equipment and Chemicals for the Laboratory 677\u003c\/p\u003e \u003cp\u003eIndex 685\u003c\/p\u003e  \u003cp\u003e\u003cb\u003eChristine K. F. Hermann, PhD \u003c\/b\u003eis Professor and Chair of the Department of Chemistry, Radford University, Radford, Virginia, USA.   \u003c\/p\u003e\u003cp\u003e\u003cb\u003eA comprehensive introduction to the identification of unknown organic compounds\u003c\/b\u003e \u003c\/p\u003e\u003cp\u003eIdentifying unknown compounds is one of the most important parts of the study of chemistry. From basic characteristics such as melting and\/or boiling point to more complex data generated through cutting-edge techniques, the range of possible methods for identifying unknown organic compounds is substantial. The utility of a research reference which compiles known techniques and characteristics of possible compounds is clear. \u003c\/p\u003e\u003cp\u003e\u003ci\u003eThe Systematic Identification of Organic Compounds \u003c\/i\u003eprovides such a reference, designed to teach a hands-on approach in the chemistry lab. It takes readers step-by-step through the process of identifying an unknown compound and elucidating its structure from infrared, nuclear magnetic resonance, and mass spectra in addition to solubility characteristics, melting point, boiling point, and classification tests. The result is an essential overview for advanced chemistry students looking to understand this exciting area of laboratory work. \u003c\/p\u003e\u003cp\u003eReaders of the ninth edition of \u003ci\u003eThe Systematic Identification of Organic Compounds \u003c\/i\u003ewill also find: \u003c\/p\u003e\u003cul\u003e\n\u003cli\u003e A detailed chapter on safety, personal protection equipment, chemical storage, safety data sheets, and other safety concerns\u003c\/li\u003e \u003cli\u003e New NMR, IR, and mass spectra with detailed explanations on interpretation\u003c\/li\u003e \u003cli\u003e Questions at the end of each chapter designed to facilitate and reinforce progression, keyed to a companion website for instructors\u003c\/li\u003e \u003cli\u003e Tables of known compounds including data relevant for identification\u003c\/li\u003e \u003cli\u003e Companion website with structural problems from experimental data for students to practice how to reason and solve\u003c\/li\u003e\n\u003c\/ul\u003e \u003cp\u003e\u003ci\u003eThe Systematic Identification of Organic Compounds \u003c\/i\u003eis\u003ci\u003e \u003c\/i\u003ea useful reference for advanced undergraduates and graduate students studying organic chemistry, organic spectroscopy, and related subjects.\u003c\/p\u003e","brand":"Wiley","offers":[{"title":"Default Title","offer_id":47990350971109,"sku":"NP9781119799665","price":111.0,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9781119799665.jpg?v=1761787469","url":"https:\/\/k12savings.com\/products\/the-systematic-identification-of-organic-compounds-isbn-9781119799665","provider":"K12savings","version":"1.0","type":"link"}