{"product_id":"organic-syntheses-volume-94-isbn-9781119511946","title":"Organic Syntheses, Volume 94","description":"The current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products. \u003cp\u003e\u003cb\u003ePreparation of Aryl Alkyl Ketenes 1\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eNicholas D. Staudaher, Joseph Lovelace, Michael P. Johnson, and Janis Louie\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of Diisopropylammonium Bis(catecholato)cyclohexylsilicate 16\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eKingson Lin, Christopher B. Kelly, Matthieu Jouffroy, and Gary A.Molander\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eContinuous Flow Hydration of Pyrazine-2-carbonitrile in a Manganese Dioxide Column Reactor 34\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eClaudio Battilocchio, Shing-Hing Lau, Joel M. Hawkins, and Steven V. Ley\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e\u003ci\u003eSite-Selective C-H Fluorination of Pyridines and Diazines with AgF\u003csub\u003e2\u003c\/sub\u003e 46\u003cbr\u003e\u003c\/i\u003e\u003c\/b\u003e\u003ci\u003ePatrick S. Fier and John F. Hartwig\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSite-Selective C-H Fluorination of Pyridines and Diazines with AgF2 46\u003cbr\u003e\u003c\/b\u003e\u003ci\u003ePatrick S. Fier and John F. Hartwig\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eUgi Multicomponent Reaction 54\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eAndré Boltjes, Haixia Liu, Haiping Liu, and Alexander Dömling\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePalladium-catalyzed External-CO-Free Reductive Carbonylation of Bromoarenes 66\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eHideyuki Konishi, Masataka Fukuda, Tsuyoshi Ueda, and Kei Manabe\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePractical Syntheses of [2,2′-bipyridine]\u003ci\u003ebis\u003c\/i\u003e[3,5-difluoro-2- [5-(trifluoromethyl)-2 pyridinyl]phenyl]iridium(III) hexafluorophosphate, [Ir{dF(CF3)ppy}2(bpy)]PF6 and [4,4′-\u003ci\u003ebis\u003c\/i\u003e (tert-butyl) 2,2′-bipyridine]\u003ci\u003ebis\u003c\/i\u003e[3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl]phenyl]iridium(III) hexafluorophosphate, [Ir{dF(CF\u003csub\u003e3\u003c\/sub\u003e)ppy}\u003csub\u003e2\u003c\/sub\u003e (dbbpy)]PF\u003csub\u003e6\u003c\/sub\u003e 77\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eMartins S. Oderinde and Jeffrey W. Johannes \u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e(Z)-Enol \u003ci\u003ep\u003c\/i\u003e-Tosylate Derived from Methyl Acetoacetate: A Useful Cross-coupling Partner for the Synthesis of Methyl (\u003ci\u003eZ\u003c\/i\u003e)-3-Phenyl (or Aryl)-2-butenoate 93\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eYuichiro Ashida, Hidefumi Nakatsuji, and Yoo Tanabe\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSynthesis of Allenyl Mesylate by a Johnson-Claisen Rearrangement. Preparation of 3-(((tert-butyldiphenyl- silyl)oxy)methyl)penta-3,4-dien-1-yl methanesulfonate 109\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eJoseph E. Burchick. Jr., Sarah M. Wells, and Kay M. Brummond\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eRhodium(I)-catalyzed Allenic Pauson–Khand Reaction 123\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eJoseph E. Burchick. Jr., Sarah M. Wells, and Kay M. Brummond\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eDirhodium (II) tetrakis[N-4-bromo-1,8-naphthoyl-(S)-\u003ci\u003etert\u003c\/i\u003e-leucinate] 136\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eHélène Lebel, Henri Piras, and Johan Bartholoméüs\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eButa-2,3-dien-1-ol 153\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eHongwen Luo, Dengke Ma, and Shengming Ma\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eFragment Coupling and Formation of Quaternary Carbons by Visible-Light Photoredox Catalyzed Reaction of \u003ci\u003etert\u003c\/i\u003e-Alkyl Hemioxalate Salts and Michael Acceptors 167\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eChristopher R. Jamison, Yuriy Slutskyy, and Larry E. Overman\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e\u003ci\u003eN-\u003c\/i\u003eMethoxy\u003ci\u003e-N-\u003c\/i\u003emethylcyanoformamide 184\u003ci\u003e\u003cbr\u003e\u003c\/i\u003e\u003c\/b\u003e\u003ci\u003eJeremy Nugent and Brett D. Schwartz\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4-Cyano-2-methoxybenzenesulfonyl Chloride 198\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eElliott D. Bayle, Niall Igoe, and Paul V. Fish\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of \u003ci\u003eN\u003c\/i\u003e-Trifluoromethylthiosaccharin: A Shelf-Stable Electrophilic Reagent for Trifluoromethylthiolation 217\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eJiansheng Zhu, Chunhui Xu, Chunfa Xu, and Qilong Shen\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eHomologation of Boronic Esters with Lithiated Epoxides 234\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eRoly J. Armstrong and Varinder K. Aggarwal\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eAsymmetric Michael Reaction of Aldehydes and Nitroalkenes 252\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eYujiro Hayashi and Shin Ogasawara\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of \u003ci\u003eanti\u003c\/i\u003e-1,3-Amino Alcohol Derivatives Through an Asymmetric Aldol-Tishchenko Reaction of Sulfinimines 259\u003cbr\u003e\u003c\/b\u003e\u003ci\u003ePamela Mackey, Rafael Cano, Vera M. Foley, and Gerard P. McGlacken\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eRhenium-Catalyzed \u003ci\u003eortho\u003c\/i\u003e-Alkylation of Phenols 280\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eYoichiro Kuninobu, Masaki, Yamamoto, Mitsumi Nishi, Tomoyuki Yamamoto, Takashi Matsuki, Masahito Murai, and Kazuhiko Takai\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eEnantioselective Preparation of 5-Oxo-5,6-dihydro-2H-pyran-2-yl phenylacetate via organocatalytic Dynamic Kinetic Asymmetric Transformation (DyKAT) 292\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eTamas Benkovics, Adrian Ortiz, Gregory L. Beutner, and Chris Sfouggatakis\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of Sodium Heptadecyl Sulfate (\u003ci\u003eTergitol-7i\u003c\/i\u003e) 303\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eBrent A. Banasik and Mansour Samadpour\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eCatalytic Enantioselective Addition of Diethyl Phosphite to N-Thiophosphinoyl Ketimines: Preparation of (\u003ci\u003eR\u003c\/i\u003e)-Diethyl (1-Amino-1-phenylethyl)phosphonate 313\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eShaoquan Lin, Yasunari Otsuka, Liang Yin, Naoya Kumagai, and Masakatsu Shibasaki\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eWater-promoted, Open-flask Synthesis of Amine-boranes: 2-Methylpyridine-borane (2-Picoline-borane) 332\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eAmeya S. Kulkarni and P. Veeraraghavan Ramachandran\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of N-Sulfinyl Aldimines using Pyrrolidine as Catalyst \u003ci\u003evia\u003c\/i\u003e Iminium Ion Activation 346\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eSara Morales, Alfonso García Rubia, Eduardo Rodrigo, José Luis Aceña, José Luis García Ruano, and M. Belén Cid\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSynthesis of \u003ci\u003eN\u003c\/i\u003e-Boc-\u003ci\u003eN\u003c\/i\u003e-Hydroxymethyl-L-phenylalaninal 358\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eJae Won Yoo, Youngran Seo, Dongwon Yoo, and Young Gyu Kim\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSynthesis of Methyl \u003ci\u003etrans\u003c\/i\u003e-Oxazolidine-5-carboxylate, a Chiral Synthon for threo-β-Amino-α-hydroxy Acid 372\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eYoungran Seo, Jae Won Yoo, Yoonjae Lee, Boram Lee, Bonghyun Kim, and Young Gyu Kim\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of Benzyl((\u003ci\u003eR\u003c\/i\u003e)-2-(4-(benzyloxy)phenyl)-2-((tert- butoxycarbonyl)amino)acetyl)-D-phenylalaninate using Umpolung Amide Synthesis 388\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eMatthew T. Knowe, Sergey V. Tsukanov, and Jeffrey N. Johnston\u003c\/i\u003e\u003c\/p\u003e  \u003cp\u003e\u003cstrong\u003eMargaret M. Faul\u003c\/strong\u003e received her B.Sc. and M.Sc degrees from University College Dublin, Ireland. She then moved to the US where she received her Ph.D. degree in synthetic organic chemistry from Harvard University with Professor David A. Evans. In 1993 Margaret joined the Chemical Process group at Eli Lilly and Company, and in 2003 she moved to Amgen where she is currently the Executive Director in the Process Development organization. At Amgen, Margaret is responsible for the commercial process development and process characterization of all molecules in both the synthetic and biologic Amgen portfolio.\u003c\/p\u003e","brand":"Wiley","offers":[{"title":"Default Title","offer_id":47989734179045,"sku":"NP9781119511946","price":210.95,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9781119511946.jpg?v=1761785294","url":"https:\/\/k12savings.com\/products\/organic-syntheses-volume-94-isbn-9781119511946","provider":"K12savings","version":"1.0","type":"link"}