{"product_id":"organic-syntheses-volume-93-isbn-9781119349020","title":"Organic Syntheses, Volume 93","description":"\u003cp\u003eThe current volume continues the tradition of the \u003cb\u003eOrganic Syntheses\u003c\/b\u003e series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.\u003c\/p\u003e \u003cp\u003e\u003cb\u003eDIBALH-Mediated Reductive Ring-Expansion Reaction of Cyclic Ketoxime 1\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eTaku Imaizumi, Kentaro Okano, and Hidetoshi Tokuyama\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of 2-(2-(Dicyclohexylphosphino)phenyl)-1-methyl-1\u003c\/b\u003e\u003cb\u003e\u003ci\u003eH\u003c\/i\u003e\u003c\/b\u003e\u003cb\u003e-indole (CM-phos) 14\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eShun Man Wong, On Ying Yuen, Pui Ying Choy, Chau Ming So, and Fuk Yee Kwong\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSynthesis of 5-(Hydroxymethyl)furfural (HMF) 29\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eSvilen P. Simeonov, Jaime A. S. Coelho, and Carlos A. M. Afonso\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e\u003ci\u003eErratum for: \u003c\/i\u003e\u003c\/b\u003e\u003cb\u003eTitanium-Mediated Addition of Silyl Dienol Ethers to Electrophilic Glycine: 4 Ketopipecolic Acid Hydrochloride 37\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eClarisse Mühlemann, Peter Hartmann, and Jean-Pierre Obrecht\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eNickel-Catalyzed Synthesis of Ketones from Alkyl Halides and Acid Chlorides: Preparation of Ethyl 4-Oxododecanoate 50\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eAlexander C. Wotal, Donald C. Batesky, and Daniel J. Weix\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eTrichloroboron-promoted Deprotection of Phenolic Benzyl Ether UsingPentamethylbenzene as a Non Lewis-Basic Cation Scavenger 63\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eShun Okaya, Keiichiro Okuyama, Kentaro Okano, and Hidetoshi Tokuyama\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eEnantioselective Synthesis of \u003c\/b\u003eα\u003cb\u003e,\u003c\/b\u003eα\u003cb\u003e-Disubstituted Lactones via a Chiral Brønsted Acid-Catalyzed Intramolecular Cyclization 75\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eJennifer E. Wilent, Ghassan Qabaja, and Kimberly S. Petersen\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eEnantioselective Synthesis of \u003c\/b\u003eα\u003cb\u003e-Bromonitroalkanes for Umpolung Amide Synthesis: Preparation of \u003c\/b\u003e\u003cb\u003e\u003ci\u003etert\u003c\/i\u003e\u003c\/b\u003e\u003cb\u003e-Butyl ((1\u003c\/b\u003e\u003cb\u003e\u003ci\u003eR\u003c\/i\u003e\u003c\/b\u003e\u003cb\u003e)-1-(4-(benzyloxy)phenyl)-2-bromo-2-nitroethyl)carbamate 88\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eVictoria T. Lim, Sergey V. Tsukanov, Amanda B. Stephens, and Jeffrey N. Johnston\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSynthesis of 1-Bromopyrene and 1-Pyrenecarbaldehyde 100\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eMatthias Schulze, Alexander Scherer, Colin Diner, and Rik R. Tykwinski\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eIntermolecular [2+2] Cycloaddition of Alkynes with Alkenes Catalyzed by Gold(I) 115\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eM. Elena de Orbe and Antonio M. Echavarren\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePhotochemical Benzannulation of \u003c\/b\u003e\u003cb\u003e\u003ci\u003eN\u003c\/i\u003e\u003c\/b\u003e\u003cb\u003e-Phosphoryl Ynamides and \u003c\/b\u003eα\u003cb\u003e-Diazo Ketones in Continuous Flow 127\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eJohn M. Read, Yu-Pu Wang, and Rick L. Danheiser\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eTrifluoromethylation of Aryl Iodides Catalyzed by the Copper(I)-Phen Complex 147\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eNaoto Shimizu, Hideaki Kondo, Masahiro Oishi, Kenichi Fujikawa, Kazuki Komoda, \u003c\/i\u003e\u003ci\u003eand Hideki Amii\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eCopper-catalyzed Cyanation of Alkenyl Iodides 163\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eAntoine Nitelet, Sara Zahim, Cédric Theunissen, Alexandre Pradal, and Gwilherm Evano\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eVisible Light Photocatalysis of Radical Cation Diels–Alder Cycloadditions: Preparation of Tris(2,2’-bipyrazyl) Ruthenium(II) Bis(tetrakis(3,5-bis(trifluoromethyl)phenyl)borate) 178\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eShane D. Lies, Shishi Lin, and Tehshik P. Yoon\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of Methyl 1,2,3,4-tetra-\u003c\/b\u003e\u003cb\u003e\u003ci\u003eO\u003c\/i\u003e\u003c\/b\u003e\u003cb\u003e-acetyl-\u003c\/b\u003eβ\u003cb\u003e-D-glucopyranuronate 200\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eAisling Ní Cheallaigh, Garrett T. Potter, John M. Gardiner, and Gavin J. Miller\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of 1,5-Dioxaspiro[5.5]undecan-3-one 210\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eRobert A. Craig, II, Russell C. Smith, Beau P. Pritchett, Benzi I. Estipona, and \u003c\/i\u003e\u003ci\u003eBrian M. Stoltz\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eOxyboration: Synthesis of Borylated Benzofurans 228\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eDarius J. Faizi, Nicole A. Nava, Mohammad Al-Amin, and Suzanne A. Blum\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSynthesis of 1-Iodopropyne 245\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eSamuel G. Bartko, James Deng, and Rick L. Danheiser\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePotassium \u003c\/b\u003e\u003cb\u003e\u003ci\u003etert\u003c\/i\u003e\u003c\/b\u003e\u003cb\u003e-Butoxide–Catalyzed Dehydrogenative Cross-Coupling of Heteroarenes with Hydrosilanes 263\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eAnton A. Toutov, Wen-Bo Liu, Brian M. Stoltz, and Robert H. Grubbs\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSynthesis of \u003c\/b\u003eα\u003cb\u003e-Carboline 272\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eLinli He, Shawn P. Allwein, Benjamin J. Dugan, Kyle W. Knouse, Gregory R. Ott, and \u003c\/i\u003e\u003ci\u003eCraig A. Zificsak\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSynthesis of Methyl 1-Formylcyclopropanecarboxylate utilizing Ti-Claisen Condensation 286\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eYuichiro Ashida, Satomi Kajimoto, Hidefumi Nakatsuji, and Yoo Tanabe\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eNickel-Catalyzed Suzuki–Miyaura Coupling in \u003c\/b\u003e\u003cb\u003e\u003ci\u003et\u003c\/i\u003e\u003c\/b\u003e\u003cb\u003e-Amyl Alcohol for the Preparation of 5-(Furan-3-\u003c\/b\u003e\u003cb\u003eyl)pyrimidine 306\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eLiana Hie and Neil K. Garg\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of (S)-Nonafluorobutanesulfinamide 319\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eApiwat Wangweerawong, Scott Kolmar, and Jonathan A. Ellman\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of 1-Methylimidazole-\u003c\/b\u003e\u003cb\u003e\u003ci\u003eN\u003c\/i\u003e\u003c\/b\u003e\u003cb\u003e-oxide (NMI-O) 331\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eJames I. Murray and Alan C. Spivey\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePalladium-Catalyzed Direct Amination of Allylic Alcohols at Room Temperature 341\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eBao Gao, Lixin Li, Guoying Zhang, and Hanmin Huang\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePreparation of 1,1-Difluoroallenes by Difluorovinylidenation of Carbonyl Compounds 352\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eKohei Fuchibe, Masashi Abe, Ken Oh, and Junji Ichikawa\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eRhodium-Catalyzed Addition of Carboxylic Acids to Terminal Alkynes towards \u003c\/b\u003e\u003cb\u003e\u003ci\u003eZ\u003c\/i\u003e\u003c\/b\u003e\u003cb\u003e-Enol Esters 367\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eStephanie Ganss, Julia Pedroni, Alexandre Lumbroso, Günther Leonhardt-Lutterbeck, \u003c\/i\u003e\u003ci\u003eAntje Meißner, Siping Wei, Hans-Joachim Drexler, Detlef Heller, and Bernhard Breit\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eCopper-Catalyzed Semi-Reduction of Alkynes 385\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eNick Cox, Hester Dang, Aaron M. Whittaker, and Gojko Lalic\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSynthesis of Cyclobutanes by Lewis Acid-Promoted Ketene-Alkene [2+2] Cycloadditions 401\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eChristopher M. Rasik, Eleni M. Salyers, and M. Kevin Brown\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSynthesis of 2,2-Dichloroimidazolidine-4,5-diones and their Application in Chlorodehydroxylation 413\u003cbr\u003e\u003c\/b\u003e\u003ci\u003eDavid Schilter and Christopher W. Bielawski\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eHuw M. L. Davies, PhD, joined the Emory University faculty in 2008 as the Asa Griggs Candler Professor of Organic Chemistry. Prior to Emory, he held the positions of UB Distinguished Professor and Larkin Professor of Organic Chemistry at the University at Buffalo, the State University of New York. Dr. Davies received his BSc degree from University College in Cardiff, Wales and his PhD from the University of East Anglia. He completed his post-doctoral training at Princeton University.\u003c\/p\u003e","brand":"Wiley","offers":[{"title":"Default Title","offer_id":47989734146277,"sku":"NP9781119349020","price":218.95,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9781119349020.jpg?v=1761785294","url":"https:\/\/k12savings.com\/products\/organic-syntheses-volume-93-isbn-9781119349020","provider":"K12savings","version":"1.0","type":"link"}