{"product_id":"organic-syntheses-volume-86-isbn-9780470556146","title":"Organic Syntheses, Volume 86","description":"The current volume continues the tradition of providing significant and interesting procedures, which should prove worthwhile to many synthetic chemists working in increasingly diverse areas. Following precedent, there is no specific or central theme to this volume.  Preparation of (3,5-Dimethoxy-1-Phenyl Cyclohexa-2,5-Dienyl)-Acetonitrile Through Birch Reductive Alkylation (BRA) (\u003ci\u003eRaphael Lebeuf, Muriel Berlande, Frédéric Robert, and Yannick Landais)\u003c\/i\u003e.  \u003cp\u003eSynthesis of Tert-Butyl (1S,2S)-2-Methyl-3-Oxo-1-Phenylpropylcarbamate By Asymmetric Mannich Reaction (\u003ci\u003eJung Woon Yang, Subhas Chandra, Pan, and Benjamin List\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eSynthesis of Pyrazolo[1,5-a]Pyridines Via Azirines: Preparation of 2-(3-Bromophenyl)-6-(Trifluoromethyl)Pyrazolo[1,5-a]Pyridine (\u003ci\u003eStephen Greszler and Kirk L. Stevens\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eBenzyl Alcohol as an Alkylating Agent Using the Ruthenium-Catalyzed Borrowing Hydrogen Strategy (\u003ci\u003eTracy D. Nixon, Paul A. Slatford, Michael K. Whittlesey and Jonathan M. J. Williams\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003e2-(2,2-Dibromoethenyl)-Benzenamine (\u003ci\u003eChristopher Bryan, Valentina Aurregi and Mark Lautens\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003e(S)-(-)-2-Allylcyclohexanone (\u003ci\u003eManfred Braun, Panos Meletis, and Mesut Fidan\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003ePreparation of 4-Spirocyclohexyloxazolidinone By C-H Bond Nitrene Insertion (\u003ci\u003eKim Huard and Hélène Lebel\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003ePreparation of (S)-4-Isopropyl-N-Propanoyl-1,3-Thiazolidine-2-Thione (\u003ci\u003eErik Gálvez, Pedro Romea, and Felix Urpi\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eStereoselective Synthesis of Anti α-Methyl-ß-Methoxy Carboxylic Compounds (\u003ci\u003eErik Gálvez, Pedro Romea, and Fèlix Urpi\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eSynthesis of 2-Arylindole-4-Carboxylic Amides: [2-(4-Fluorophenyl)-1H-Indol-4-YL]-1-Pyrrolidinylmethanone (\u003ci\u003eJeffrey T. Kuethe and Gregory L. Beutner\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003ePalladium (II) Acetate-Butyldi-1- Adamantylphosphine Catalyzed Arylation of Electron-Rich Heterocycles. Preparation of 5-Phenyl-2-Isobutylthiazole (\u003ci\u003eAnna Lazareva, Hendrich A. Chiong, and Olafs Daugulis\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eMild and Efficient One-Pot Curtius Rearrangement: Preparatino of N-Tert-Butyl Adamantanyl-1-YL-Carbamate (\u003ci\u003eOlivier Leogane and Hélène Lebel\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eEnantioselective Oxidation of An Alkyl Aryl Sulfide: Synthesis of (S)-(-) Methyl p-Bromophenyl Sulfoxide (\u003ci\u003eCarmelo Drago, Emma-Hane Walker, Lorenzo Caggiano and Richard F. W. Jackson\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eProtection of Diols with 4-(tert-Butyldimethylsilyloxy)Benzylidene Acetal and Its Deprotection:(4-((4R,5R)-4,5-Diphenyl-1,3-Dioxolan-2-YL) Phenoxy) (Tert-Butyl)Dimethylsilane (\u003ci\u003eHiroyuki Osajima, Hideto Fujiwara, Kentaro Okano, Hidetoshi Tokuyama, and Tohru Fukuyama\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eSynthesis of 2-[3,3'-DI-(\u003ci\u003eTert\u003c\/i\u003e-Butoxycarbonyl)-Aminodipropylamine]-4,6,-Dichloro-1,3,5-[Tris-Piperazine]-Triazine As a Core for the Large Scale Syntehsis of Melamine (Triazine) Dendrimers (\u003ci\u003eAbdellatif Chouai, Vincent J. Venditto, and Eric E. Simanek\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eLarge Scale, Green Syntehsis of a Generation-1 Melamine (Triazine) Dendrimer) (\u003ci\u003eAbdellatif Chouai, Vincent J. Venditto, and Eric E. Simanek\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eThe Direct Acyl-Alkylation of Arynes. Preparation of Methyl 2-(2-Acetylphenyl) Acetate (\u003ci\u003eDavid C. Ebner, Uttam K. Tambar, and Brian M. Stoltz\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eConvenient Preparation of 3-Ethoxycarbonyl Benzofurans From Salicylaldehydes adn Ethyl Diazoacetate (\u003ci\u003eMatthew E. Dudley, M. Monzur Morshed, and M. Mahmun Hossain\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003ePreparation of (S)-Tert-Butylphon (\u003ci\u003eMichael R. Krout, Justin T. Mohr, and Brian M. Stoltz\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003ePreparation of (S)-2-Allyl-2-Methylcyclohexanone (\u003ci\u003eJustin T. Mohr, Michael R. Krout, and Brian M. Stoltz\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003ePhosphine-Catalyzed [4+2] Annulation: Synthesis of Ethyl 6-Phenyl-1-Tosyl-1,2,5,6-Tetrahydropyridine-3-Carboxylate (\u003ci\u003eKui Lu and Ohyun Kwon\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eSyntehsis of Polyynes by In Situ Desilylative Brominatino and Palladium-Catalyzed Coupling: (7-(Benzyloxy)Hepta-1,3,5-Triynyl) Triisopropylsilane (\u003ci\u003eSoonho Hwang, Hee Ryong Kang, and Sanghee Kim\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eEnantioselective Preparation of Dihydropyrimidones (\u003ci\u003eJennifer M. Goss, Peng Dai, Sha Lou, and Scott E. Schaus\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eOne-Pot Multicomponent Preparation of Tetrahydropyrzaoloquinolinones and Tetrahydropyrazoloquinazolinones (\u003ci\u003eToma N. Glasnov and C. Oliver Kape\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003e (3R,7aS)-3-(Trichloromethyl)Tetrahydropyrrolo[1,2-C]Oxazol-1(3H)-One: An Air and Moisture Stable Reagent For the Synthesis of Optically Active α-Branched Prolines (\u003ci\u003eGareld D. Artmann III, Ryan J. Rafferty, and Rovert M. Williams\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eVinylation with Inexpensive Silicon-Based Reagents: Preparation of 3-Vinylquinoline and 4-Vinylbenzophenone (\u003ci\u003eScott E. Denmark and Christophe R. Butler\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eLow Pressure Carbonylation of Epoxides to ß-Lactones (\u003ci\u003eJohn W. Kramer, Daniel S. Treitler, and Geoffrey W. Coates\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eTetrakis(Dimethylamino)Allene (\u003ci\u003eAlois Fürstner, Manuel Alcarazo, and Helga Krause\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eEfficient One-Pot Synthesis of Bis(4-Tert-Butylphenyl)Iodonium Triflate (\u003ci\u003eMarcin Bielawski and Berit Olofsson\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003ePd(0)-Catalyzed Diamination of Trans-1-Phenyl-1,3-Butadiene with Di-Tert-butyldiaziridinone As Nitrogen Source (\u003ci\u003eHaifeng Du, Baoguo Zhao, and Yian Shi\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eSynthesis of Ethyl 2-Ethanoyl-2-Methyl-3-Phenylbut-3-Enoate (\u003ci\u003eTaisuke Fujimoto, Kohei Endo, Masaharu Nakamura, and Eiichi Nakamura\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eSynthesis of 4,5-Dimethyl-1,3-Dithiol-2-One (\u003ci\u003ePerumalreddy Chandreasekaran and James P. Donahue\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eB-Protected Haloboronic Acids For Iterative Cross-Coupling (\u003ci\u003eSteven G. Ballmer, Eric P. Gillis, and Martin D. Burke\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eRhodium-Catalyzed Enantioselective Addition of Arylboronic Acids to In Situ Generated N-Boc Arylimines. Preparatin of (S)-Tert-Butyl (4-Chlorophenyl) (Thiophen-2-YL)Methylcarbamate (\u003ci\u003eMorten Storgaard and Jonathan A. Ellman\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003eMagnesiation of Weakly Activated Arenes Using tmp\u003csub\u003e2\u003c\/sub\u003eMg 2LiC1:Synthesis of Tert-Butyl Ethyl Phthalate (\u003ci\u003eChristoph J. Rohbogner, Andreas J. Wagner, Giuliano C. Clososki, and Paul Knochel\u003c\/i\u003e).\u003c\/p\u003e \u003cp\u003e\u003cb\u003eERRATA.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e1,4-BIS(Trimethylsilyl)Buta-1,3-Diyne (\u003ci\u003eGraham E. Jones, David A. Kendrick, and Andrew B. Holmes\u003c\/i\u003e).\u003c\/p\u003e  \u003cp\u003eJohn A. Ragan is the author of Organic Syntheses, Volume 86, published by Wiley.\u003c\/p\u003e","brand":"Wiley","offers":[{"title":"Default Title","offer_id":47989733785829,"sku":"NP9780470556146","price":102.95,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9780470556146.jpg?v=1761785293","url":"https:\/\/k12savings.com\/products\/organic-syntheses-volume-86-isbn-9780470556146","provider":"K12savings","version":"1.0","type":"link"}