{"product_id":"nmr-of-quadrupolar-nuclei-in-solid-materials-isbn-9780470973981","title":"NMR of Quadrupolar Nuclei in Solid Materials","description":"\u003cb\u003eNMR OF QUADRUPOLAR NUCLEI IN SOLID MATERIALS\u003c\/b\u003e \u003cp\u003eOver the past 20 years technical developments in superconducting magnet technology and instrumentation have increased the potential of NMR spectroscopy so that it is now possible to study a wide range of solid materials. In addition, one can probe the nuclear environments of many other additional atoms that possess the property of spin. In particular, it is possible to carry out NMR experiments on isotopes that have nuclear spin greater that ½ (i.e. quadrupolar nuclei). Since more that two-thirds of all NMR active isotopes are quadrupolar nuclei, applications of NMR spectroscopy with quadrupolar nuclei are increasing rapidly. \u003c\/p\u003e\u003cp\u003eThe purpose of this handbook is to provide under a single cover the fundamental principles, techniques and applications of quadrupolar NMR as it pertains to solid materials. Each chapter has been prepared by an expert who has made significant contributions to out understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three sections: The first provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar neclei in solids. The second presents cutting-edge techniques and methodology for employing these techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of dynamics, characterizations of biological samples, organic and inorganic materials, porous materials, glasses, catalysts, semiconductors and high-temperature superconductors. \u003c\/p\u003e\u003cp\u003e\u003cb\u003eAbout EMR Handbooks\u003c\/b\u003e \u003c\/p\u003e\u003cp\u003eThe \u003ci\u003eEncyclopedia of Magnetic Resonance (EMR)\u003c\/i\u003e publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence-of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of Encyclopedia articles. In consultation with the EMR Editorial Board, the EMR Handbooks are coherently planned in advance by ­specially-selected Editors, and new articles, are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in ­academia or industry. \u003c\/p\u003e\u003cp\u003eHave the content of this handbook and the complete content of the Encyclopedia of Magnetic Resonance at your fingertips! \u003c\/p\u003e\u003cp\u003eVisit: \u003cb\u003ewww.wileyonlinelibrary.com\/ref\/emr\u003c\/b\u003e \u003c\/p\u003e\u003cp\u003eContributors ix\u003c\/p\u003e \u003cp\u003eSeries Preface xiii\u003c\/p\u003e \u003cp\u003eVolume Preface xv\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePart A: Basic Principles 1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e1 Quadrupolar Interactions\u003cbr\u003e \u003ci\u003ePascal P. Man 3\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e2 Quadrupolar Nuclei in Solids\u003cbr\u003e \u003ci\u003eAlexander J. Vega 17\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e3 Quadrupolar Coupling: An Introduction and Crystallographic Aspects\u003cbr\u003e \u003ci\u003eSharon E. Ashbrook, Stephen Wimperis 45\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e4 Quadrupolar Nuclei in Solids: Influence of Different Interactions on Spectra\u003cbr\u003e \u003ci\u003eDavid L. Bryce, Roderick E. Wasylishen 63\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePart B: Advanced Techniques 75\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e5 Acquisition of Wideline Solid-State NMR Spectra of Quadrupolar Nuclei\u003cbr\u003e \u003ci\u003eRobert W. Schurko 77\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e6 Sensitivity and Resolution Enhancement of Half-Integer Quadrupolar Nuclei in Solid-State NMR\u003cbr\u003e \u003ci\u003eThomas T. Nakashima, Roderick E. Wasylishen 95\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e7 Quadrupolar Nutation Spectroscopy\u003cbr\u003e \u003ci\u003eArno P.M. Kentgens 107\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e8 Dynamic Angle Spinning\u003cbr\u003e \u003ci\u003ePhilip J. Grandinetti 121\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e9 Double Rotation (DOR) NMR\u003cbr\u003e \u003ci\u003eRay Dupree 133\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e10 MQMAS NMR: Experimental Strategies\u003cbr\u003e \u003ci\u003eJean-Paul Amoureux, Marek Pruski 143\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e11 STMAS NMR: Experimental Advances\u003cbr\u003e \u003ci\u003eSharon E. Ashbrook, Stephen Wimperis 163\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e12 Correlation Experiments Involving Half-Integer Quadrupolar Nuclei\u003cbr\u003e \u003ci\u003eMichael Deschamps, Dominique Massiot 179\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e13 Computing Electric Field Gradient Tensors\u003cbr\u003e \u003ci\u003eJosef W. Zwanziger 199\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePart C: Applications 211\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e14 Quadrupolar NMR to Investigate Dynamics in Solid Materials\u003cbr\u003e \u003ci\u003eLuke A. O’Dell, Christopher I. Ratcliffe 213\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e15 Alkali Metal NMR of Biological Molecules\u003cbr\u003e \u003ci\u003eGang Wu 233\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e16 Nitrogen-14 NMR Studies of Biological Systems\u003cbr\u003e \u003ci\u003eLuminita Duma 255\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e17 Oxygen-17 NMR Studies of Organic and Biological Molecules\u003cbr\u003e \u003ci\u003eGang Wu 273\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e18 Oxygen-17 NMR of Inorganic Materials\u003cbr\u003e \u003ci\u003eSharon E. Ashbrook, Mark E. Smith 291\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e19 Chlorine, Bromine, and Iodine Solid-State NMR\u003cbr\u003e \u003ci\u003eDavid L. Bryce, Cory M. Widdifield, Rebecca P. Chapman, Robert J. Attrell 321\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e20 Quadrupolar NMR of Ionic Conductors, Batteries, and other Energy-Related Materials\u003cbr\u003e \u003ci\u003eFrédéric Blanc, Leigh Spencer, Gillian R. Goward 349\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e21 Quadrupolar NMR of Nanoporous Materials\u003cbr\u003e \u003ci\u003eMohamed Haouas, Charlotte Martineau, Francis Taulelle 371\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e22 Quadrupolar NMR in the Earth Sciences\u003cbr\u003e \u003ci\u003eJonathan F. Stebbins 387\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e23 Quadrupolar NMR of Superconductors\u003cbr\u003e \u003ci\u003eNicholas J. Curro 401\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e24 Quadrupolar NMR of Semiconductors\u003cbr\u003e \u003ci\u003eJames P. Yesinowski 417\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e25 Quadrupolar NMR of Metal Nuclides in Biological Materials\u003cbr\u003e \u003ci\u003eTatyana Polenova, Andrew S. Lipton, Paul D. Ellis 439\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e26 Nuclear Waste Glasses: Insights from Solid-State NMR\u003cbr\u003e \u003ci\u003eScott Kroeker 453\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e27 Quadrupolar Metal NMR of Oxide Materials Including Catalysts\u003cbr\u003e \u003ci\u003eOlga B. Lapina, Victor V. Terskikh 467\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e28 Quadrupolar NMR of Intermetallic Compounds\u003cbr\u003e \u003ci\u003eFrank Haarmann 495\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eIndex 511\u003c\/p\u003e  \u003cp\u003e\u003cb\u003eRoderick E. Wasylishen\u003c\/b\u003e, Canada Research Chair in Physical Chemistry, Department of ­Chemistry, Edmonton, Alberta, Canada. \u003c\/p\u003e\u003cp\u003e\u003cb\u003eSharon E. Ashbrook\u003c\/b\u003e, Reader, School of Chemistry, University of St Andrews, UK. \u003c\/p\u003e\u003cp\u003e\u003cb\u003eStephen Wimperis\u003c\/b\u003e, Professor, Department of Chemistry, Faculty of Physical Sciences, ­University of Glasgow, UK.   \u003c\/p\u003e\u003cp\u003eOver the past 20 years technical developments in superconducting magnet technology and instrumentation have increased the potential of NMR spectroscopy so that it is now possible to study a wide range of solid materials. In addition, one can probe the nuclear environments of many other additional atoms that possess the property of spin. In particular, it is possible to carry out NMR experiments on isotopes that have nuclear spin greater that ½ (i.e. quadrupolar nuclei). Since more that two-thirds of all NMR active isotopes are quadrupolar nuclei, applications of NMR spectroscopy with quadrupolar nuclei are increasing rapidly. \u003c\/p\u003e\u003cp\u003eThe purpose of this handbook is to provide under a single cover the fundamental principles, techniques and applications of quadrupolar NMR as it pertains to solid materials. Each chapter has been prepared by an expert who has made significant contributions to out understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three sections: The first provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar neclei in solids. The second presents cutting-edge techniques and methodology for employing these techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of dynamics, characterizations of biological samples, organic and inorganic materials, porous materials, glasses, catalysts, semiconductors and high-temperature superconductors. \u003c\/p\u003e\u003cp\u003e\u003cb\u003eAbout EMR Handbooks\u003c\/b\u003e \u003c\/p\u003e\u003cp\u003eThe \u003ci\u003eEncyclopedia of Magnetic Resonance (EMR)\u003c\/i\u003e publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence-of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of Encyclopedia articles. In consultation with the EMR Editorial Board, the EMR Handbooks are coherently planned in advance by ­specially-selected Editors, and new articles, are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in ­academia or industry. \u003c\/p\u003e\u003cp\u003eHave the content of this handbook and the complete content of the Encyclopedia of Magnetic Resonance at your fingertips! \u003c\/p\u003e\u003cp\u003eVisit: \u003cb\u003ewww.wileyonlinelibrary.com\/ref\/emr\u003c\/b\u003e\u003c\/p\u003e","brand":"Wiley","offers":[{"title":"Default Title","offer_id":47989692301541,"sku":"NP9780470973981","price":193.95,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9780470973981.jpg?v=1761785124","url":"https:\/\/k12savings.com\/products\/nmr-of-quadrupolar-nuclei-in-solid-materials-isbn-9780470973981","provider":"K12savings","version":"1.0","type":"link"}