Microscale Organic Laboratory

Microscale Organic Chemistry: With Multistep and Multiscale Syntheses offers a modern approach to the laboratory experience within the organic division. Notable features include inquiry-driven experimentation, validation of the purification process, and the implementation of greener processes (including microwave use) to perform traditional experimentation. In addition to offering alternative methods to perform microscale experiments, this text offers strong pedagogy to promote student success through empowerment and encouragement.

Chapter 1 Introduction 1

Chapter 2 Safety 6

Chapter 3 Introduction to Microscale Organic Laboratory Equipment And Techniques 20

Chapter 4 Determination of Physical Properties 47

Chapter 5 Microscale Laboratory Techniques 59

Chapter 6 Microscale Organic Laboratory Experiments 119

Chapter 7 Sequential Syntheses: the Transition From Macro To Micro 440

Chapter 8 Spectroscopic Identification The Monochromator 625

Chapter 9 Qualitative Identification Of Organic Compounds 649

Chapter 10 Advanced Microscale Organic Laboratory Experiments 685

Glossary G-1

Index I-1