{"product_id":"handbook-of-high-field-dynamic-nuclear-polarization-isbn-9781119441649","title":"Handbook of High Field Dynamic Nuclear Polarization","description":"\u003cp\u003e\u003cb\u003eAddresses Dynamic Nuclear Polarization (DNP) as a technique for sensitivity-enhancement in solid-state NMR spectroscopy\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eThis comprehensive handbook is a compendium of the current state-of-the art of high field Dynamic Nuclear Polarization—from long-proven, early developments, up to today’s hot topics. It covers all the relevant subjects that have made a direct or indirect contribution toward advancing this field, and focuses on topics such as: the theory behind the effects seen within DNP; instrumentation required for carrying out DNP; and specific applications of DNP including protein monitoring, catalysis, nanoparticles, biological and clinical studies. Development and application of techniques that have indirectly contributed to advancing MAS DNP NMR, such as DNP experiments on static solids within microwave resonant structures, and high-field EPR, are also examined.\u003c\/p\u003e \u003cp\u003e\u003ci\u003eHandbook of High Field Dynamic Nuclear Polarization\u003c\/i\u003e is presented in three sections—Theoretical Aspects, DNP Development (instrumentation \/ radical \/ sample), and DNP NMR Applications. The first section offers chapters on; solid and cross effect DNP; thermal mixing; Overhauser; and dissolution DNP. The second looks at: microwave technology, gyrotron, and IOE; homebuilt and commercial DNP spectrometers; and glassing vs. solvent-free DNP. The final section provides information on; amyloid, membrane, and nanocrystalline proteins; metals, and surface enhanced DNP; pharmaceuticals; nanoparticles; and much more. \u003c\/p\u003e \u003cul\u003e \u003cli\u003eCovers one of the biggest developing fields in magnetic resonance\u003c\/li\u003e \u003cli\u003eRelevant to students, academics, and industry within the physical, materials, medical, and biochemical sciences\u003c\/li\u003e \u003cli\u003eAn excellent starting point and point-of-reference for researchers in the field\u003c\/li\u003e \u003cli\u003eEdited by a widely respected team with contributions from key researchers in the NMR community\u003c\/li\u003e \u003cli\u003ePart of the \u003ci\u003eeMagRes\u003c\/i\u003e Handbook Series\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003ci\u003eHandbook of High Field Dynamic Nuclear Polarization\u003c\/i\u003e is an ideal reference for all researchers and graduate students involved in this complex, interdisciplinary field.\u003c\/p\u003e \u003cp\u003e\u003cb\u003eAbout eMagRes Handbooks \u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003ci\u003eeMagRes\u003c\/i\u003e publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of \u003ci\u003eeMagRes\u003c\/i\u003e Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of \u003ci\u003eeMagRes\u003c\/i\u003e articles. In consultation with the \u003ci\u003eeMagRes\u003c\/i\u003e Editorial Board, the \u003ci\u003eeMagRes\u003c\/i\u003e Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.\u003c\/p\u003e \u003cp\u003eHave the content of this Handbook and the complete content of \u003ci\u003eeMagRes\u003c\/i\u003e at your fingertips!\u003c\/p\u003e \u003cp\u003eVisit: www.wileyonlinelibrary.com\/ref\/eMagRes\u003c\/p\u003e \u003cp\u003eContributors xi\u003c\/p\u003e \u003cp\u003eSeries Preface xvii\u003c\/p\u003e \u003cp\u003ePreface xix\u003c\/p\u003e \u003cp\u003eAcknowledgments xxi\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePart A: Concepts, Theory, \u0026amp; Instrumentation 1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e1 The Discovery and Demonstration of Dynamic Nuclear Polarization–A Personal and Historical Account 3\u003cbr\u003e\u003ci\u003eCharles P. Slichter\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e2 DNP Mechanisms 15\u003cbr\u003e\u003ci\u003eKrishnendu Kundu, Frédéric Mentink-Vigier, Akiva Feintuch, and Shimon Vega\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e3 Pulsed Dynamic Nuclear Polarization 71\u003cbr\u003e\u003ci\u003eKong Ooi Tan, Sudheer Jawla, Richard J. Temkin, and Robert G. Griffin\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e4 MAS-DNP Enhancements: Hyperpolarization, Depolarization, and Absolute Sensitivity 87\u003cbr\u003e\u003ci\u003eSabine Hediger, Daniel Lee, Frédéric Mentink-Vigier, and Gaël De Paëpe\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e5 Polarizing Agents: Evolution and Outlook in Free Radical Development for DNP 103\u003cbr\u003e\u003ci\u003eGilles Casano, Hakim Karoui, and Olivier Ouari\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e6 Paramagnetic Metal Ions for Dynamic Nuclear Polarization 121\u003cbr\u003e\u003ci\u003eBjörn Corzilius\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e7 Instrumentation for High-field Dynamic Nuclear Polarization NMR Spectroscopy 143\u003cbr\u003e\u003ci\u003eGuy M. Bernard and Vladimir K. Michaelis\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e8 Millimeter-wave Sources for DNP-NMR 155\u003cbr\u003e\u003ci\u003eMonica Blank and Kevin L. Felch\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e9 Cryogenic Platforms and Optimized DNP Sensitivity 169\u003cbr\u003e\u003ci\u003eYoh Matsuki and Toshimichi Fujiwara\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e10 Versatile Dynamic Nuclear Polarization Hardware with Integrated Electron Paramagnetic Resonance Capabilities 189\u003cbr\u003e\u003ci\u003eAlisa Leavesley, Ilia Kaminker, and Songi Han\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e11 Dissolution Dynamic Nuclear Polarization Methodology and Instrumentation 219\u003cbr\u003e\u003ci\u003eDennis Kurzbach and Sami Jannin\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e12 Introduction to Dissolution DNP: Overview, Instrumentation, and Human Applications 239\u003cbr\u003e\u003ci\u003eJan H. Ardenkjaer-Larsen\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e13 Liquid-state Overhauser DNP at High Magnetic Fields 261\u003cbr\u003e\u003ci\u003eVasyl P. Denysenkov and Thomas F. Prisner\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e14 Overhauser DNP in Liquids on 13C Nuclei 279\u003cbr\u003e\u003ci\u003eMarina Bennati and Tomas Orlando\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePart B: Applications 289\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e15 DNP and Cellular Solid-state NMR 291\u003cbr\u003e\u003ci\u003eAlessandra Lucini Paioni, Marie A.M. Renault, and Marc Baldus\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e16 Cryo-trapped Intermediates of Retinal Proteins Studied by DNP-enhanced MAS NMR Spectroscopy 305\u003cbr\u003e\u003ci\u003eJohanna Becker-Baldus and Clemens Glaubitz\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e17 DNP Solid-state NMR of Biological Membranes 323\u003cbr\u003e\u003ci\u003eBurkhard Bechinger\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e18 DNP in Materials Science: Touching the Surface 337\u003cbr\u003e\u003ci\u003ePierrick Berruyer, Lyndon Emsley, and Anne Lesage\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e19 Growing Signals from the Noise: Challenging Nuclei in Materials DNP 353\u003cbr\u003e\u003ci\u003eFrédéric A. Perras, Takeshi Kobayashi, and Marek Pruski\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e20 DNP-enhanced Solid-state NMR Spectroscopy of Active Pharmaceutical Ingredients 373\u003cbr\u003e\u003ci\u003eLi Zhao, Arthur C. Pinon, Lyndon Emsley, and Aaron J. Rossini\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e21 In Vivo Hyperpolarized 13C MRS and MRI Applications 405\u003cbr\u003e\u003ci\u003eIrene Marco-Rius and Arnaud Comment\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e22 Dissolution Dynamic Nuclear Polarization 421\u003cbr\u003e\u003ci\u003eWalter Köckenberger\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eIndex 435\u003c\/p\u003e  \u003cp\u003e\u003cb\u003eEditors\u003c\/b\u003e \u003c\/p\u003e\u003cp\u003e\u003cb\u003eVladimir K. Michaelis\u003c\/b\u003e \u003ci\u003eis Assistant Professor in the Department of Chemistry at the University of Alberta.\u003c\/i\u003e \u003c\/p\u003e\u003cp\u003e\u003cb\u003eRobert G. Griffin\u003c\/b\u003e \u003ci\u003eis Professor of Chemistry and Director of the Francis Bitter Magnet Laboratory at the Massachusetts Institute of Technology.\u003c\/i\u003e \u003c\/p\u003e\u003cp\u003e\u003cb\u003eBjörn Corzilius\u003c\/b\u003e \u003ci\u003eis Professor of Physical Chemistry in the Institute of Chemistry at the University of Rostock.\u003c\/i\u003e \u003c\/p\u003e\u003cp\u003e\u003cb\u003eShimon Vega\u003c\/b\u003e \u003ci\u003eis Professor in the Department of Chemical Physics at the Weizmann Institute of Science, Israel.\u003c\/i\u003e   \u003c\/p\u003e\u003cp\u003e\u003cb\u003eHANDBOOK OF HIGH FIELD DYNAMIC NUCLEAR POLARIZATION\u003c\/b\u003e \u003c\/p\u003e\u003cp\u003e\u003cb\u003eAddresses Dynamic Nuclear Polarization (DNP) as a technique for sensitivity-enhancement in solid-state NMR spectroscopy\u003c\/b\u003e \t \u003c\/p\u003e\u003cp\u003eThis comprehensive handbook is a compendium of the current state-of-the art of high field Dynamic Nuclear Polarization—from long-proven, early developments, up to today's hot topics. It covers all the relevant subjects that have made a direct or indirect contribution toward advancing this field, and focuses on topics such as: the theory behind the effects seen within DNP; instrumentation required for carrying out DNP; and specific applications of DNP including protein monitoring, catalysis, nanoparticles, biological and clinical studies. Development and application of techniques that have indirectly contributed to advancing MAS DNP NMR, such as DNP experiments on static solids within microwave resonant structures, and high-field EPR, are also examined. \u003c\/p\u003e\u003cp\u003e\u003ci\u003eHandbook of High Field Dynamic Nuclear Polarization\u003c\/i\u003e is presented in two sections — Concepts, Theory, \u0026amp; Instrumentation and Applications. The first section includes chapters on: solid and cross effect DNP; thermal mixing; Overhauser; cryogenic platforms; dissolution DNP; homebuilt and commercial DNP spectrometers. The second section provides information on: amyloid, membrane, and nanocrystalline proteins; metals and surface enhanced DNP; pharmaceuticals; nanoparticles; and much more. \u003c\/p\u003e\u003cul\u003e \u003cli\u003eCovers one of the biggest developing fields in magnetic resonance\u003c\/li\u003e \u003cli\u003eRelevant to students, academics, and industry within the physical, materials, medical, and biochemical sciences\u003c\/li\u003e \u003cli\u003eAn excellent starting point and point-of-reference for researchers in the field\u003c\/li\u003e \u003cli\u003eEdited by a widely respected team with contributions from key researchers in the NMR community\u003c\/li\u003e \u003cli\u003ePart of the \u003ci\u003eeMagRes\u003c\/i\u003e Handbook Series\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003ci\u003eHandbook of High Field Dynamic Nuclear Polarization\u003c\/i\u003e is an ideal reference for all researchers and graduate students involved in this complex, interdisciplinary field. \u003c\/p\u003e\u003cp\u003e\u003cb\u003eAbout \u003ci\u003eeMagRes\u003c\/i\u003e Handbooks\u003c\/b\u003e \u003c\/p\u003e\u003cp\u003e\u003ci\u003eeMagRes\u003c\/i\u003e publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of \u003ci\u003eeMagRes\u003c\/i\u003e Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of \u003ci\u003eeMagRes\u003c\/i\u003e articles. In consultation with the\u003ci\u003e eMagRes\u003c\/i\u003e Editorial Board, the \u003ci\u003eeMagRes\u003c\/i\u003e Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. \u003c\/p\u003e\u003cp\u003eHave the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com\/ref\/eMagRes\u003c\/p\u003e","brand":"Wiley","offers":[{"title":"Default Title","offer_id":47989333786853,"sku":"NP9781119441649","price":134.95,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9781119441649.jpg?v=1761783707","url":"https:\/\/k12savings.com\/products\/handbook-of-high-field-dynamic-nuclear-polarization-isbn-9781119441649","provider":"K12savings","version":"1.0","type":"link"}