{"product_id":"glow-discharge-plasmas-in-analytical-spectroscopy-isbn-9780471606994","title":"Glow Discharge Plasmas in Analytical Spectroscopy","description":"Glow discharge devices have been utilized as spectrochemical sources for over one hundred years, dating back to the earliest studies of atomic structures. It has only been during the last 40 years that they have been employed in the arena of chemical analysis. Glow Discharge Plasmas in Analytical Spectroscopy presents the state of the art in the use of these devices across a wide range of applications, including materials science, environmental analysis, and bioanalytical chemistry. Glow discharge devices are well known for their application in direct solids elemental analysis of metals and alloys by optical and mass spectrometries. These basic capabilities have been extended to the analysis of non-conducting materials such as glass and ceramics and the depth resolved analysis of all kinds of technical materials.\u003cbr\u003e This multi-author, edited volume includes chapters which deal with both basic and highly complex applications. Glow discharge devices are now being used in very novel ways for the analysis of liquids and gases, including molecular species detection and identification, an area that was beyond the perceived scope of applicability just ten years ago. It is expected that the next decade will see a growth in the interest and application of glow discharge devices far surpassing the expectations of the last century.Gegenstand des Bandes ist die Anwendung von Glimmentladungsplasmen in der analytischen Spektroskopie, insbesondere der Atomemissions-Spektroskopie und Massenspektrometrie.\u003cbr\u003e - Sammlung von Beiträgen international renommierter Fachleute\u003cbr\u003e - Herausgeber gehört zu den bekanntesten Persönlichkeiten seines Faches\u003cbr\u003e - einziges Buch auf dem Markt, das einen wirklich umfassenden Überblick über die aktuelle Forschung auf diesem Gebiet gibt\u003cbr\u003e - behandelt sowohl AES als auch MS mit Glimmentladungsplasmen \u003cp\u003ePreface xi\u003c\/p\u003e \u003cp\u003eList of Contributors xiii\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1 Introduction 1\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eR. K. Marcus and J. A. C. Broekaert\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e1.1 Rationale 1\u003c\/p\u003e \u003cp\u003e1.2 Glow Discharge Devices: Basic Operating Principles 3\u003c\/p\u003e \u003cp\u003e1.3 Glow Discharge Devices: Scope of Application 6\u003c\/p\u003e \u003cp\u003e1.4 Volume Outline 7\u003c\/p\u003e \u003cp\u003e1.5 References 12\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2 Optical Emission Spectrometry with Glow Discharges 15\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eJ. A. C. Broekaert\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e2.1 Introduction 15\u003c\/p\u003e \u003cp\u003e2.2 Glow Discharges 16\u003c\/p\u003e \u003cp\u003e2.3 Atomic Emission Spectrometry 36\u003c\/p\u003e \u003cp\u003e2.4 Material Ablation 49\u003c\/p\u003e \u003cp\u003e2.5 Analyses with Glow Discharge Atomic Emission Spectrometry 55\u003c\/p\u003e \u003cp\u003e2.6 Other Methods of Analysis and Outlook 63\u003c\/p\u003e \u003cp\u003e2.7 References 67\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3 Mass Spectrometry of Glow Discharges 71\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eW. W. Harrison, C. Yang and E. Oxley\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e3.1 Introduction 71\u003c\/p\u003e \u003cp\u003e3.2 Fundamentals of Mass Spectrometry 75\u003c\/p\u003e \u003cp\u003e3.3 Instrumentation 82\u003c\/p\u003e \u003cp\u003e3.4 Qualitative Considerations 91\u003c\/p\u003e \u003cp\u003e3.5 Quantitative Analysis 92\u003c\/p\u003e \u003cp\u003e3.6 Conclusions 95\u003c\/p\u003e \u003cp\u003e3.7 References 95\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4 Radio Frequency Glow Discharges 97\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eR. K. Marcus\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e4.1 Introduction 97\u003c\/p\u003e \u003cp\u003e4.2 Radio Frequency Glow Discharge (rf-GD) Operation Principles 99\u003c\/p\u003e \u003cp\u003e4.3 Comparisons with dc-Powered Glow Discharge Sources 101\u003c\/p\u003e \u003cp\u003e4.4 Instrumentation 106\u003c\/p\u003e \u003cp\u003e4.5 Analytical Applications 112\u003c\/p\u003e \u003cp\u003e4.6 Summary 136\u003c\/p\u003e \u003cp\u003e4.7 References 136\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5 Depth Profile Analysis 141\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eA. Bengtson\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e5.1 Introduction 141\u003c\/p\u003e \u003cp\u003e5.2 Instrumentation 142\u003c\/p\u003e \u003cp\u003e5.3 Practical Aspects and Results 144\u003c\/p\u003e \u003cp\u003e5.4 Conclusions 153\u003c\/p\u003e \u003cp\u003e5.5 References 154\u003c\/p\u003e \u003cp\u003e\u003cb\u003e6 Numerical Modeling of Analytical Glow Discharges 155\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eA. Bogaerts and R. Gijbels\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e6.1 Introduction 155\u003c\/p\u003e \u003cp\u003e6.2 Description of the Models 157\u003c\/p\u003e \u003cp\u003e6.3 Results and Discussion 170\u003c\/p\u003e \u003cp\u003e6.4 Conclusion 202\u003c\/p\u003e \u003cp\u003e6.5 References 203\u003c\/p\u003e \u003cp\u003e\u003cb\u003e7 Application of Glow Discharge Optical Emission Spectrometry in the Steel Industry 207\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eK. Kakita\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e7.1 Introduction 207\u003c\/p\u003e \u003cp\u003e7.2 Measurement Traceability of Coating Weight and Chemical Composition by GD-OES 208\u003c\/p\u003e \u003cp\u003e7.3 Method of Coating Analysis by GD-OES 209\u003c\/p\u003e \u003cp\u003e7.4 Depth Profiles of Coatings by GD-OES 213\u003c\/p\u003e \u003cp\u003e7.5 Factors Affecting Depth Profiles 217\u003c\/p\u003e \u003cp\u003e7.6 Validation and Verification of Calibration Graphs 225\u003c\/p\u003e \u003cp\u003e7.7 References 229\u003c\/p\u003e \u003cp\u003e\u003cb\u003e8 Surfaces, Thin Films and Coatings 231\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eR. Payling, P. Chapon, K. Shimizu, R. Passetemps, A. Jadin, Y. Bourgeois, K. Crener, M. Aeberhard and J. Michler\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e8.1 Introduction 231\u003c\/p\u003e \u003cp\u003e8.2 Surfaces 232\u003c\/p\u003e \u003cp\u003e8.3 Thin Films 238\u003c\/p\u003e \u003cp\u003e8.4 Coatings 243\u003c\/p\u003e \u003cp\u003e8.5 Conclusions 251\u003c\/p\u003e \u003cp\u003e8.6 Acknowledgements 251\u003c\/p\u003e \u003cp\u003e8.7 References 251\u003c\/p\u003e \u003cp\u003e\u003cb\u003e9 Comparison of Glow Discharge Atomic Spectrometry with Other Surface Analysis Methods 253\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eK. Wagatsuma\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e9.1 Introduction 253\u003c\/p\u003e \u003cp\u003e9.2 Surface Analysis Methods Competitive with Glow Discharge Spectrometry 256\u003c\/p\u003e \u003cp\u003e9.3 Analytical Examples 263\u003c\/p\u003e \u003cp\u003e9.4 References 272\u003c\/p\u003e \u003cp\u003e\u003cb\u003e10 Analysis of Samples of Nuclear Concern with Glow Discharge Atomic Spectrometry 273\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eM. Betti\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e10.1 Introduction 273\u003c\/p\u003e \u003cp\u003e10.2 Instrumentation 274\u003c\/p\u003e \u003cp\u003e10.3 Practical Aspects and Results 277\u003c\/p\u003e \u003cp\u003e10.4 Conclusions 288\u003c\/p\u003e \u003cp\u003e10.5 Acknowledgements 289\u003c\/p\u003e \u003cp\u003e10.6 References 290\u003c\/p\u003e \u003cp\u003e\u003cb\u003e11 Analysis of Nonconducting Materials by dc Glow Discharge Spectrometry 293\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eA. Bogaerts, W. Schelles and R. Van Grieken\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e11.1 Introduction 293\u003c\/p\u003e \u003cp\u003e11.2 Use of a Conducting Host Matrix 294\u003c\/p\u003e \u003cp\u003e11.3 Use of a Conducting Secondary Cathode 301\u003c\/p\u003e \u003cp\u003e11.4 Conclusion 311\u003c\/p\u003e \u003cp\u003e11.5 References 314\u003c\/p\u003e \u003cp\u003e\u003cb\u003e12 Standards and Reference Materials for Glow Discharge Spectroscopies 317\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eM. R. Winchester\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e12.1 Introduction 317\u003c\/p\u003e \u003cp\u003e12.2 Practical Aspects 318\u003c\/p\u003e \u003cp\u003e12.3 Conclusions 331\u003c\/p\u003e \u003cp\u003e12.4 References 332\u003c\/p\u003e \u003cp\u003e\u003cb\u003e13 Analysis of Liquid Samples Using Glow Discharge Spectroscopies 335\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eR. K. Marcus\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e13.1 Introduction 335\u003c\/p\u003e \u003cp\u003e13.2 Instrumentation 336\u003c\/p\u003e \u003cp\u003e13.3 Practical Aspects and Applications 341\u003c\/p\u003e \u003cp\u003e13.4 References 360\u003c\/p\u003e \u003cp\u003e14 GC Speciation with GDMS Detection 363\u003c\/p\u003e \u003cp\u003eJ. A. Caruso and L. Milstein\u003c\/p\u003e \u003cp\u003e14.1 Introduction 363\u003c\/p\u003e \u003cp\u003e14.2 Elemental Speciation 364\u003c\/p\u003e \u003cp\u003e14.3 Instrumentation 364\u003c\/p\u003e \u003cp\u003e14.4 Practical Aspects and Results 370\u003c\/p\u003e \u003cp\u003e14.5 Conclusions 378\u003c\/p\u003e \u003cp\u003e14.6 References 379\u003c\/p\u003e \u003cp\u003e\u003cb\u003e15 Glow Discharge Atomic Emission Spectrometry for the Analysis of Gases and as an Alternative Gas Chromatographic Detector 381\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eR. Pereiro, N. G. Orellana-Velado and A. Sanz-Medel\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e15.1 Introduction 381\u003c\/p\u003e \u003cp\u003e15.2 Instrumentation for the Analysis of Gases and Gas Chromatographic Detection by GD-AES 386\u003c\/p\u003e \u003cp\u003e15.3 Practical Aspects and Results 392\u003c\/p\u003e \u003cp\u003e15.4 Conclusions 399\u003c\/p\u003e \u003cp\u003e15.5 References 399\u003c\/p\u003e \u003cp\u003e\u003cb\u003e16 Low-pressure Inductively Coupled Plasmas 401\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eH. Evans\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e16.1 Introduction 401\u003c\/p\u003e \u003cp\u003e16.2 Fundamentals 403\u003c\/p\u003e \u003cp\u003e16.3 Instrumentation 407\u003c\/p\u003e \u003cp\u003e16.4 Practical Aspects and Results 416\u003c\/p\u003e \u003cp\u003e16.5 Conclusions 430\u003c\/p\u003e \u003cp\u003e16.6 References 430\u003c\/p\u003e \u003cp\u003e\u003cb\u003e17 Multidimensional Ionization Sources for Plasma-source Mass Spectrometry 435\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eJ. P. Guzowski, Jr and G. M. Hieftje\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e17.1 Introduction 435\u003c\/p\u003e \u003cp\u003e17.2 Tandem Sources in PSMS 437\u003c\/p\u003e \u003cp\u003e17.3 Multipurpose Ionization Sources for PSMS 441\u003c\/p\u003e \u003cp\u003e17.4 Conclusions 463\u003c\/p\u003e \u003cp\u003e17.5 Acknowledgments 463\u003c\/p\u003e \u003cp\u003e17.6 References 464\u003c\/p\u003e \u003cp\u003eIndex 469\u003c\/p\u003e \"...very valuable for those interested in this rapidly expanding and diagnostically important area.\"\u003cbr\u003e Journal of the American Chemical Society\u003cbr\u003e Vol. 125, NO. 39\u003cbr\u003e Born in 1948, \u003cb\u003eJosé Broekaert\u003c\/b\u003e studied chemistry at the University of Gent, Belgium, graduating in 1970. After receiving his PhD from the University of Gent in 1976 and a stay in Germany as Alexander-von-Humboldt postdoctoral fellow the following year, he was a scientist at the ISAS, Dortmund from 1978 to 1991 and obtained the degree of \"Geaggregeerde voor het hoger onderwijs\" from the University of Antwerp, Belgium in 1985. He became associate professor at the University of Dortmund in 1991, full professor at the University of Leipzig in 1998 and, in 2002, joined the University of Hamburg. In 1998 he was a visiting Fulbright research scholar at Indiana University, Bloomington, USA. His main research interests include the development of plasma optical emission, atomic absorption and inorganic mass spectrometry methods and their application in solving analytical problems. Glow discharge devices have been utilized as spectrochemical sources for over one hundred years, dating back to the earliest studies of atomic structures. It has only been during the last 40 years that they have been employed in the arena of chemical analysis. Glow Discharge Plasmas in Analytical Spectroscopy presents the state of the art in the use of these devices across a wide range of applications, including materials science, environmental analysis, and bioanalytical chemistry. Glow discharge devices are well known for their application in direct solids elemental analysis of metals and alloys by optical and mass spectrometries. These basic capabilities have been extended to the analysis of non-conducting materials such as glass and ceramics and the depth resolved analysis of all kinds of technical materials.\u003cbr\u003e \u003cbr\u003e This multi-author, edited volume includes chapters which deal with both basic and highly complex applications. Glow discharge devices are now being used in very novel ways for the analysis of liquids and gases, including molecular species detection and identification, an area that was beyond the perceived scope of applicability just ten years ago. It is expected that the next decade will see a growth in the interest and application of glow discharge devices far surpassing the expectations of the last century.","brand":"Wiley","offers":[{"title":"Default Title","offer_id":47989300560101,"sku":"NP9780471606994","price":507.95,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9780471606994.jpg?v=1761783578","url":"https:\/\/k12savings.com\/products\/glow-discharge-plasmas-in-analytical-spectroscopy-isbn-9780471606994","provider":"K12savings","version":"1.0","type":"link"}