{"product_id":"gc-ms-of-biologically-and-environmentally-significant-organic-compounds-isbn-9781119611349","title":"GC-MS of Biologically and Environmentally Significant Organic Compounds","description":"\u003cp\u003e\u003cb\u003eProvides a comprehensive guide to the use of gas chromatography–mass spectrometry (GC\u003c\/b\u003e\u003cb\u003e-\u003c\/b\u003e\u003cb\u003eMS) on environmentally significant organic compounds\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eThis book presents a library of mass spectra of 1,725 biologically and environmentally important organic compounds, in the form of their trimethylsilyl derivatives (TMS), as well as their linear temperature programmed chromatographic retention indices, \u003ci\u003eRI,\u003c\/i\u003e whose values are in the range of 700-4700 index units. Of the compounds presented, more than 60% of compounds have not previously been characterized by their mass spectra, and more than 70% not previously been characterized by their \u003ci\u003eRI\u003c\/i\u003e values. Some of these compounds, never before analysed via MS and GC, were detected by the author’s team in plant tissues.\u003c\/p\u003e \u003cp\u003eThe first chapters of the book are devoted to the methodology and practice of sample preparation, as well as to mass spectrometry considerations. They contain the discussion of possible complications and limitations of the method. The book includes lists of chemical compounds in alphabetical order, as well as in the order of their retention indices which facilitates the search for parameters of interest. Every compound in the book includes a \u003ci\u003eRI\u003c\/i\u003e value, mass spectrum, CAS number (if available), molecular and structural formula, formula weight, chemical name and list of synonyms, as well the source of compounds used for registration of spectrum and \u003ci\u003eRI\u003c\/i\u003e value.\u003c\/p\u003e \u003cul\u003e \u003cli\u003eFeatures mass spectra and chromatographic retention indices of 1,725 organic substances in the form of their trimethylsilyl derivatives (TMS)\u003c\/li\u003e \u003cli\u003eIncludes the CAS number, molecular and structural formula, formula weight, mass spectrum, chemical name and list of synonyms, and more for every compound covered within\u003c\/li\u003e \u003cli\u003eThe first publication containing analytical parameters of high-boiling compounds such as glycosides, lignans, and phenylpropenoid glycerides with \u003ci\u003eRI\u003c\/i\u003e values \u0026gt;4000\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003ci\u003eGC-MS of Biologically and Environmentally Significant Organic Compounds\u003c\/i\u003e will appeal to specialists in phytochemical analysis, food, and environmental chemistry, as well as other investigators dealing with GC or GC\/MS analysis complex mixtures of organic compounds.\u003cbr\u003e\u003cbr\u003eThe accompanying electronic database, \"Biologically and Environmentally Important Organic Compounds - GCMS Library\", will be published in mid-2020, ISBN: 978-1-119-60170-8.\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003ePreface vii\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1 Introduction \u003c\/b\u003e\u003cb\u003e1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2 Gas Chromatography and Mass Spectrometry Considerations \u003c\/b\u003e\u003cb\u003e7\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e2.1 Silylation Reagents and Procedure of Derivatisation 7\u003c\/p\u003e \u003cp\u003e2.2 Two-Step Derivatisation: Oximating−Silylating 8\u003c\/p\u003e \u003cp\u003e2.3 Analytical Procedure 10\u003c\/p\u003e \u003cp\u003e2.3.1 Selection of Stationary Phase and Conditions of Separation 10\u003c\/p\u003e \u003cp\u003e2.3.2 Sample Preparation 10\u003c\/p\u003e \u003cp\u003e2.3.3 Qualitative MS Identification 12\u003c\/p\u003e \u003cp\u003e2.3.3.1 Aliphatic Alcohols 16\u003c\/p\u003e \u003cp\u003e2.3.3.2 Aromatic Alcohols 16\u003c\/p\u003e \u003cp\u003e2.3.3.3 Carboxylic Acids 16\u003c\/p\u003e \u003cp\u003e2.3.3.4 Amino Acids 16\u003c\/p\u003e \u003cp\u003e2.3.3.5 Phenylpropanoids 17\u003c\/p\u003e \u003cp\u003e2.3.3.6 Flavonoids 18\u003c\/p\u003e \u003cp\u003e2.3.3.7 Steroids 20\u003c\/p\u003e \u003cp\u003e2.3.3.8 Carbohydrates and Glycosides 22\u003c\/p\u003e \u003cp\u003e2.4 A Critical Role of Retention Indices in GS–MS Investigations 24\u003c\/p\u003e \u003cp\u003e2.5 Experimental Factors Influencing the Accuracy of Retention Indices 28\u003c\/p\u003e \u003cp\u003e2.6 Possible Artefacts and Complications of Mass Spectral Identification 30\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3 Explanation of Format Used in the Book \u003c\/b\u003e\u003cb\u003e33\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4 References \u003c\/b\u003e\u003cb\u003e35\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5 Alphabetic Listing of Compounds \u003c\/b\u003e\u003cb\u003e43\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e6 Compounds Listed in Order of Their Retention Indices \u003c\/b\u003e\u003cb\u003e87\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e7 Mass Spectra and Retention Indices of TMS Derivatives \u003c\/b\u003e\u003cb\u003e131\u003c\/b\u003e\u003c\/p\u003e  \u003cp\u003e\u003cb\u003eVALERY A. ISIDOROV, P\u003csmall\u003eH\u003c\/small\u003eD, Dr Sci\u003c\/b\u003e is Professor at Bialystok University of Technology, Poland, specializing in analytical chemistry, environmental chemistry, and the chemistry of natural products.   \u003c\/p\u003e\u003cp\u003e\u003cb\u003eProvides a comprehensive guide to the use of gas chromatography–mass spectrometry (GC-MS) on environmentally significant organic compounds\u003c\/b\u003e \u003c\/p\u003e\u003cp\u003eThis book presents a library of mass spectra of 1,725 biologically and environmentally important organic compounds, in the form of their trimethylsilyl derivatives (TMS), as well as their linear temperature programmed chromatographic retention indices,??\u003ci\u003eRI,\u003c\/i\u003e??whose values are in the range of 700–4700 index units. Of the compounds presented, more than 60% of compounds have not previously been characterized by their mass spectra, and more than 70% not previously been characterized by their??\u003ci\u003eRI\u003c\/i\u003e??values. Some of these compounds, never before analysed via MS and GC, were detected by the author's team in plant tissues. \u003c\/p\u003e\u003cp\u003eThe first chapters of the book are devoted to the methodology and practice of sample preparation, as well as to mass spectrometry considerations. They feature a discussion of possible complications and limitations of the method. The book includes lists of chemical compounds in alphabetical order, as well as in the order of their retention indices which facilitates the search for parameters of interest. Every compound in the book includes a??\u003ci\u003eRI\u003c\/i\u003e??value, mass spectrum, CAS number (if available), molecular and structural formula, formula weight, chemical name and list of synonyms, as well the source of compounds used for registration of the spectrum and??the \u003ci\u003eRI\u003c\/i\u003e??value. \u003c\/p\u003e\u003cul\u003e \u003cli\u003eFeatures mass spectra and chromatographic retention indices of 1,725 organic substances in the form of their trimethylsilyl derivatives (TMS)\u003c\/li\u003e \u003cli\u003eIncludes the CAS number, molecular and structural formula, formula weight, mass spectrum, chemical name and list of synonyms, and more, for every compound covered\u003c\/li\u003e \u003cli\u003eThe first publication containing analytical parameters of high-boiling compounds such as glycosides, lignans, and phenylpropenoid glycerides with??\u003ci\u003eRI\u003c\/i\u003e??values \u0026gt;4000\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003ci\u003eGC-MS of Biologically and Environmentally Significant Organic Compounds\u003c\/i\u003e??will appeal to specialists in phytochemical analysis, food, and environmental chemistry, as well as other investigators dealing with GC or GC\/MS analysis complex mixtures of organic compounds.\u003c\/p\u003e","brand":"Wiley","offers":[{"title":"Default Title","offer_id":47989272838373,"sku":"NP9781119611349","price":540.95,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9781119611349.jpg?v=1761783468","url":"https:\/\/k12savings.com\/products\/gc-ms-of-biologically-and-environmentally-significant-organic-compounds-isbn-9781119611349","provider":"K12savings","version":"1.0","type":"link"}