{"product_id":"essential-methods-of-instrumental-analysis-isbn-9781394226719","title":"Essential Methods of Instrumental Analysis","description":"\u003cp\u003e\u003cb\u003eIntuitively organized textbook aligned to common analytical instrumentation courses for undergraduate students\u003c\/b\u003e \u003c\/p\u003e\u003cp\u003eThrough an analytical approach, \u003ci\u003eEssential Methods of Instrumental Analysis \u003c\/i\u003eprovides an expansive overview of common instruments and methods and their applications for undergraduate students, integrating experimental protocols with real result examples to deliver a well-rounded understanding of the inner workings of the instruments and enabling students to evaluate the success of their experiments and create scientific figures. \u003c\/p\u003e\u003cp\u003eIn addition to detailed coverage of specific instruments, the book discusses analytical laboratory practices, instrument maintenance, statistics, and real-world lab experiments with previous student results. Each analytical method section includes extensive sample preparation information, rather than a simple stand-alone chapter offering generic discussions not connected to specific methods. \u003c\/p\u003e\u003cp\u003eThis book conveniently organizes content by analyte class (inorganic and organic) in a way that is intuitive to a student and aligned with relevant courses. Ancillaries including .mp4 videos, instructor PowerPoint slides, and animations are included on a companion website. \u003c\/p\u003e\u003cp\u003eWritten by an experienced professor and tested and refined over years in his courses since 2008, \u003ci\u003eEssential Methods of Instrumental Analysis\u003c\/i\u003e includes information on sample topics such as: \u003c\/p\u003e\u003cul\u003e\n\u003cli\u003eProper laboratory protocols for analytical instrumentation, covering chemical reagents, glassware, calibration techniques, and figures of merit\u003c\/li\u003e\n\u003cli\u003eOptical physics, covering the interaction of electromagnetic radiation with instrument components and sample molecules, relaxation processes, reflection, diffraction, dispersion, and refraction\u003c\/li\u003e\n\u003cli\u003eFlame atomic absorption and flame emission spectrometry, covering optical radiation sources, mirrors, choppers, burner heads, and doppler broadening\u003c\/li\u003e\n\u003cli\u003eGas and liquid chromatography, covering gaseous, liquid, soil-sediment, and biological samples, analyte recovery, chromatography theory, injectors, columns and ovens, common detectors, and mass spectrometers\u003c\/li\u003e\n\u003c\/ul\u003e \u003cp\u003eFocusing on contrasts and comparisons across multiple types of instruments in a way distinct from similar texts, \u003ci\u003eEssential Methods of Instrumental Analysis \u003c\/i\u003eis an essential textbook for students in advanced undergraduate courses in related programs of study. \u003c\/p\u003e\u003cp\u003eAbout the Authors xv\u003c\/p\u003e \u003cp\u003ePreface xix\u003c\/p\u003e \u003cp\u003eAbout the Companion Website\u003ci\u003e xxi\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1 Proper Laboratory Protocols for Analytical Instrumentation 1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e1.1 Laboratory Preliminaries 1\u003c\/p\u003e \u003cp\u003e1.2 Standard Practices 11\u003c\/p\u003e \u003cp\u003e1.3 Questions 13\u003c\/p\u003e \u003cp\u003e1.4 Problems 14\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2 Statistical Analysis 17\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e2.1 Introduction 17\u003c\/p\u003e \u003cp\u003e2.2 Linear Least-squares Analysis 18\u003c\/p\u003e \u003cp\u003e2.3 Student’s t-test Equations 20\u003c\/p\u003e \u003cp\u003e2.4 Assignments 24\u003c\/p\u003e \u003cp\u003eFurther Reading 24\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3 A Review of Optical Physics 25\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e3.1 Introduction 25\u003c\/p\u003e \u003cp\u003e3.2 Interaction of Electromagnetic Radiation with Sample Molecules 26\u003c\/p\u003e \u003cp\u003e3.3 Interaction of Electromagnetic Radiation with Surfaces 32\u003c\/p\u003e \u003cp\u003e3.4 Detectors in UV–visible Spectrometry 41\u003c\/p\u003e \u003cp\u003e3.5 Summary 48\u003c\/p\u003e \u003cp\u003eReference 49\u003c\/p\u003e \u003cp\u003e3.6 Questions 49\u003c\/p\u003e \u003cp\u003eSupporting Information 51\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4 Analytical Molecular Spectrometry 53\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e4.1 Introduction 53\u003c\/p\u003e \u003cp\u003e4.2 Basic UV–Vis Spectrometer 53\u003c\/p\u003e \u003cp\u003e4.3 From Simple to Complex UV–Visible Spectrometers 54\u003c\/p\u003e \u003cp\u003e4.4 Fluorescence and Phosphorescence Instruments 55\u003c\/p\u003e \u003cp\u003e4.5 Instrument Maintenance 57\u003c\/p\u003e \u003cp\u003e4.6 Summary 57\u003c\/p\u003e \u003cp\u003e4.7 Case Study: Quantitation of Riboflavin by UV–Vis and Fluorescence Spectrometry by Nate Boland 60\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5 Flame Atomic Absorption and Flame Emission Spectrometry 61\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e5.1 Introduction and History of Atomic Absorption Spectrometry (AAS) 61\u003c\/p\u003e \u003cp\u003e5.2 Components of a Flame Atomic Absorption\/Emission Spectrometer System 61\u003c\/p\u003e \u003cp\u003e5.3 Specialized Sample Introduction Techniques and Analysis 73\u003c\/p\u003e \u003cp\u003e5.4 General Operation of FAAS and FAES Instruments 76\u003c\/p\u003e \u003cp\u003e5.5 Maintenance 76\u003c\/p\u003e \u003cp\u003e5.6 Summary 76\u003c\/p\u003e \u003cp\u003e5.7 Questions 77\u003c\/p\u003e \u003cp\u003eSupporting Information 78\u003c\/p\u003e \u003cp\u003e\u003cb\u003e6 Inductively Coupled Plasma 79\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e6.1 Introduction and History 79\u003c\/p\u003e \u003cp\u003e6.2 Atomic Emission Spectrometry Theory 79\u003c\/p\u003e \u003cp\u003e6.3 Components of an Inductively Coupled Plasma: Atomic Emission Spectrometry System (ICP–AES) 80\u003c\/p\u003e \u003cp\u003e6.4 Interferences 90\u003c\/p\u003e \u003cp\u003e6.5 Maintenance 90\u003c\/p\u003e \u003cp\u003e6.6 Case Study: Quantitation of Heavy Metals in Consumer Products by Dan Burgard 90\u003c\/p\u003e \u003cp\u003e6.7 Summary 91\u003c\/p\u003e \u003cp\u003e6.8 Questions 92\u003c\/p\u003e \u003cp\u003eSupporting Information 92\u003c\/p\u003e \u003cp\u003eReferences 93\u003c\/p\u003e \u003cp\u003e\u003cb\u003e7 Inductively Coupled Plasma–Mass Spectrometry 95\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e7.1 Introduction and History 95\u003c\/p\u003e \u003cp\u003e7.2 Components of a Mass Spectrometer 95\u003c\/p\u003e \u003cp\u003e7.3 Summary 112\u003c\/p\u003e \u003cp\u003e7.4 Questions 113\u003c\/p\u003e \u003cp\u003eSupporting Information 115\u003c\/p\u003e \u003cp\u003eReference 115\u003c\/p\u003e \u003cp\u003eFurther Reading 115\u003c\/p\u003e \u003cp\u003e\u003cb\u003e8 Contrasts and Comparisons of Instrumentation 117\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e8.1 Introduction 117\u003c\/p\u003e \u003cp\u003e8.2 Figures of Merit 117\u003c\/p\u003e \u003cp\u003e8.3 Questions 120\u003c\/p\u003e \u003cp\u003e\u003cb\u003e9 Chromatography Introduction, Chromatography Theory, and Instrument Calibration 121\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e9.1 Introduction 121\u003c\/p\u003e \u003cp\u003e9.2 Chromatographic Theory 122\u003c\/p\u003e \u003cp\u003e9.3 Case Study 129\u003c\/p\u003e \u003cp\u003e9.4 Optimization of Chromatographic Conditions 131\u003c\/p\u003e \u003cp\u003e9.5 Calibration of an Instrument\/Detector 133\u003c\/p\u003e \u003cp\u003e9.6 Evolution of Peak Integration 135\u003c\/p\u003e \u003cp\u003eSupporting Information 136\u003c\/p\u003e \u003cp\u003eReferences 136\u003c\/p\u003e \u003cp\u003e\u003cb\u003e10 Gas Chromatography 137\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e10.1 Introduction and History 137\u003c\/p\u003e \u003cp\u003e10.2 Types of Samples and Sample Introduction 137\u003c\/p\u003e \u003cp\u003e10.3 Gas Chromatography 143\u003c\/p\u003e \u003cp\u003e10.4 Advanced GC Systems 152\u003c\/p\u003e \u003cp\u003e10.5 Applications\/Case Studies 152\u003c\/p\u003e \u003cp\u003e10.6 Summary 160\u003c\/p\u003e \u003cp\u003e10.7 Questions 161\u003c\/p\u003e \u003cp\u003eSupporting Information 162\u003c\/p\u003e \u003cp\u003eReference 162\u003c\/p\u003e \u003cp\u003e\u003cb\u003e11 High-performance Liquid Chromatography 163\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e11.1 Introduction and History 163\u003c\/p\u003e \u003cp\u003e11.2 Types of Analytes, Samples, and Sample Introduction 165\u003c\/p\u003e \u003cp\u003e11.3 Liquid Chromatography 166\u003c\/p\u003e \u003cp\u003e11.4 Advanced and Specialty LC Systems 173\u003c\/p\u003e \u003cp\u003e11.5 Applications\/Case Studies 177\u003c\/p\u003e \u003cp\u003e11.6 Summary 180\u003c\/p\u003e \u003cp\u003e11.7 Questions 180\u003c\/p\u003e \u003cp\u003eSupporting Information 182\u003c\/p\u003e \u003cp\u003eReferences 182\u003c\/p\u003e \u003cp\u003e\u003cb\u003e12 Capillary Electrophoresis by Nicole James 185\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e12.1 Introduction 185\u003c\/p\u003e \u003cp\u003e12.2 Electrophoresis and Capillary Electrophoresis 185\u003c\/p\u003e \u003cp\u003e12.3 Samples 190\u003c\/p\u003e \u003cp\u003e12.4 Methods of Operation 192\u003c\/p\u003e \u003cp\u003e12.5 Detectors 195\u003c\/p\u003e \u003cp\u003e12.6 Application\/Case Studies 199\u003c\/p\u003e \u003cp\u003e12.7 Summary 202\u003c\/p\u003e \u003cp\u003eReferences 202\u003c\/p\u003e \u003cp\u003e\u003cb\u003e13 Mass Spectrometry 203\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e13.1 Introduction and History 203\u003c\/p\u003e \u003cp\u003e13.2 Sample Introduction from GC and Analyte Ionization 204\u003c\/p\u003e \u003cp\u003e13.3 Introduction of Samples from HPLC 210\u003c\/p\u003e \u003cp\u003e13.4 Introduction of Samples from a Capillary Electrophoresis System 214\u003c\/p\u003e \u003cp\u003e13.5 Common Mass Filters (Mass Analyzers) 216\u003c\/p\u003e \u003cp\u003e13.6 Ion Detectors 238\u003c\/p\u003e \u003cp\u003e13.7 Three-dimensional Aspects of GC–MS 239\u003c\/p\u003e \u003cp\u003e13.8 Summary 239\u003c\/p\u003e \u003cp\u003e13.9 Questions 240\u003c\/p\u003e \u003cp\u003eSupporting Information 242\u003c\/p\u003e \u003cp\u003eReferences 242\u003c\/p\u003e \u003cp\u003eFurther Reading 242\u003c\/p\u003e \u003cp\u003e\u003cb\u003e14 Fragmentation and Interpretation of Spectra 245\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e14.1 Introduction 245\u003c\/p\u003e \u003cp\u003e14.2 Creation of the Spectra 246\u003c\/p\u003e \u003cp\u003e14.3 Identifying the Molecular Ion Peak 247\u003c\/p\u003e \u003cp\u003e14.4 Use of the Molecular Ion 249\u003c\/p\u003e \u003cp\u003e14.5 Identification of Analytes Using Isotopic Ratios 252\u003c\/p\u003e \u003cp\u003e14.6 Fragmentation 255\u003c\/p\u003e \u003cp\u003e14.7 Rearrangements 257\u003c\/p\u003e \u003cp\u003e14.8 Identification of Compounds 257\u003c\/p\u003e \u003cp\u003e14.9 Fragmentation of Hydrocarbons 258\u003c\/p\u003e \u003cp\u003e14.10 Fragmentation of Alcohols 262\u003c\/p\u003e \u003cp\u003e14.11 Fragmentation of Ketones and Aldehydes 265\u003c\/p\u003e \u003cp\u003e14.12 Fragmentation of Carboxylic Acids 270\u003c\/p\u003e \u003cp\u003e14.13 Fragmentation of Ethers 271\u003c\/p\u003e \u003cp\u003e14.14 Fragmentation of Esters 273\u003c\/p\u003e \u003cp\u003e14.15 Fragmentation of Amines 276\u003c\/p\u003e \u003cp\u003e14.16 Fractionation of Amides 278\u003c\/p\u003e \u003cp\u003e14.17 Fragmentation of Nitriles 279\u003c\/p\u003e \u003cp\u003e14.18 Reviewing General Principles 280\u003c\/p\u003e \u003cp\u003e14.19 Searchable Databases 284\u003c\/p\u003e \u003cp\u003e\u003cb\u003e15 Common Radiochemical Detection Methods in Analytical Chemistry 285\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e15.1 Introduction 285\u003c\/p\u003e \u003cp\u003e15.2 Common Sources of Radiation 285\u003c\/p\u003e \u003cp\u003e15.3 Detection of Alpha, Beta, and Gamma Emission 286\u003c\/p\u003e \u003cp\u003e15.4 Case Studies 290\u003c\/p\u003e \u003cp\u003eReference 290\u003c\/p\u003e \u003cp\u003e\u003cb\u003e16 Instrumental Laboratory Experiments with Results 291\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e16.1 Introduction 291\u003c\/p\u003e \u003cp\u003e16.2 A Typical Glassware Inventory for an Instrumental Methods Course 291\u003c\/p\u003e \u003cp\u003e16.3 Maintaining a Legally Defensible Laboratory Notebook 291\u003c\/p\u003e \u003cp\u003e16.4 Solutions, Weights, and Laboratory Techniques 293\u003c\/p\u003e \u003cp\u003e16.5 Determination of a Surrogate Toxic Metal (Ca) in a Simulated Hazardous Waste Sample by a Variety of Techniques 295\u003c\/p\u003e \u003cp\u003e16.6 Identification of Components in Liquors and Distilled Spirits 306\u003c\/p\u003e \u003cp\u003e16.7 Identification of Fragrances 311\u003c\/p\u003e \u003cp\u003e16.8 GC–MS Analysis of Synthetic and Natural Fragrances by Evan Bowman, Annika Mayo, and Aurora Anderson 316\u003c\/p\u003e \u003cp\u003e16.9 SPME–GC–MS Analysis of Wine Headspace by Bailey Arend 324\u003c\/p\u003e \u003cp\u003e16.10 Quantitative Determination of the Presence of Captan on Organic and Nonorganic Strawberries by Peter Mullin, Eric Ying, Jon Na, Sharon Ndayambaje, and Soren Sandeno 330\u003c\/p\u003e \u003cp\u003e16.11 Determination of Nicotine in Human Urine Using HPLC–MS by Ashley Nguyen, Lea Molacek, Maxwell Brown 333\u003c\/p\u003e \u003cp\u003e16.12 Analysis of Caffeine in Urine Samples Using GC–FID by Elsa Nader, Ralph Huang, Aaron Lieberman, Jane Duncan, and Matt Sousa 336\u003c\/p\u003e \u003cp\u003e16.13 Caffeine in the Walla Walla (WA) Wastewater Effluent by MacKenzie Cummings, Mia Groff, Roya Nasseri, Noah Willis, and Clara Wheeler 338\u003c\/p\u003e \u003cp\u003e16.14 Gasoline Analysis by GC–FID and GC–MS by Theodore Pierce and Austin Shaff 340\u003c\/p\u003e \u003cp\u003e16.15 GC–MS as an Effective Instrument for Detecting Cocaine on US Currency by Jessica Boyers and Kacey Godwin 343\u003c\/p\u003e \u003cp\u003e16.16 Analytical Quantification of CBD-A Content in Cannabis sativa (Hemp) Using GC–FID and GC–MS by Lauren Yumibe, Sam Weiss, Maddie Bowers, Tori Li, Asher Bachtold, and Brandon Neifert 347\u003c\/p\u003e \u003cp\u003e16.17 Results and Discussion 349\u003c\/p\u003e \u003cp\u003e16.18 Conclusions 350\u003c\/p\u003e \u003cp\u003eReferences 351\u003c\/p\u003e \u003cp\u003eFurther Reading 354\u003c\/p\u003e \u003cp\u003eIndex 357\u003c\/p\u003e  \u003cp\u003e\u003cb\u003eFrank M. Dunnivant,\u003c\/b\u003e PhD is a Professor in the Department of Chemistry at Whitman College. He has worked for several labs including the Oak Ridge National Laboratory, the Idaho National Engineering Laboratory, and the University of Zurich (ETH) and the Swiss Federal Institute for Water and Waste Water Pollution (EAWAG). \u003c\/p\u003e\u003cp\u003e\u003cb\u003eJake W. Ginsbach,\u003c\/b\u003e PhD is a Principal Consultant at Kaiser Permanente. At Stanford and Whitman College, his research included lab analyses of environmental chemicals and contaminants, studying the activation of dioxygen at copper active sites in metalloenzymes, along with helping develop two e-textbooks.   \u003c\/p\u003e\u003cp\u003e\u003cb\u003eIntuitively organized textbook aligned to common analytical instrumentation courses for undergraduate students\u003c\/b\u003e \u003c\/p\u003e\u003cp\u003eThrough an analytical approach, \u003ci\u003eEssential Methods of Instrumental Analysis \u003c\/i\u003eprovides an expansive overview of common instruments and methods and their applications for undergraduate students, integrating experimental protocols with real result examples to deliver a well-rounded understanding of the inner workings of the instruments and enabling students to evaluate the success of their experiments and create scientific figures. \u003c\/p\u003e\u003cp\u003eIn addition to detailed coverage of specific instruments, the book discusses analytical laboratory practices, instrument maintenance, statistics, and real-world lab experiments with previous student results. Each analytical method section includes extensive sample preparation information, rather than a simple stand-alone chapter offering generic discussions not connected to specific methods. \u003c\/p\u003e\u003cp\u003eThis book conveniently organizes content by analyte class (inorganic and organic) in a way that is intuitive to a student and aligned with relevant courses. Ancillaries including .mp4 videos, instructor PowerPoint slides, and animations are included on a companion website. \u003c\/p\u003e\u003cp\u003eWritten by an experienced professor and tested and refined over years in his courses since 2008, \u003ci\u003eEssential Methods of Instrumental Analysis\u003c\/i\u003e includes information on sample topics such as: \u003c\/p\u003e\u003cul\u003e\n\u003cli\u003eProper laboratory protocols for analytical instrumentation, covering chemical reagents, glassware, calibration techniques, and figures of merit\u003c\/li\u003e\n\u003cli\u003eOptical physics, covering the interaction of electromagnetic radiation with instrument components and sample molecules, relaxation processes, reflection, diffraction, dispersion, and refraction\u003c\/li\u003e\n\u003cli\u003eFlame atomic absorption and flame emission spectrometry, covering optical radiation sources, mirrors, choppers, burner heads, and doppler broadening\u003c\/li\u003e\n\u003cli\u003eGas and liquid chromatography, covering gaseous, liquid, soil-sediment, and biological samples, analyte recovery, chromatography theory, injectors, columns and ovens, common detectors, and mass spectrometers\u003c\/li\u003e\n\u003c\/ul\u003e \u003cp\u003eFocusing on contrasts and comparisons across multiple types of instruments in a way distinct from similar texts, \u003ci\u003eEssential Methods of Instrumental Analysis \u003c\/i\u003eis an essential textbook for students in advanced undergraduate courses in related programs of study.\u003c\/p\u003e","brand":"Wiley","offers":[{"title":"Default Title","offer_id":47989156839653,"sku":"NP9781394226719","price":96.5,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9781394226719.jpg?v=1761783025","url":"https:\/\/k12savings.com\/products\/essential-methods-of-instrumental-analysis-isbn-9781394226719","provider":"K12savings","version":"1.0","type":"link"}