{"product_id":"application-of-ic-ms-and-ic-icp-ms-in-environmental-research-isbn-9781118862001","title":"Application of IC-MS and IC-ICP-MS in Environmental Research","description":"Introduces the reader to the field of ion chromatography, species analysis and hyphenated methods IC-MS and IC-ICP-MS including the theory and theirs applications \u003cbr\u003e \u003cul\u003e \u003cli\u003eCovers the importance of species analysis and hyphenated methods  in ion chromatography \u003c\/li\u003e \u003cli\u003eIncludes practical applications of IC-MS and IC-ICP-MS in environmental analysis\u003c\/li\u003e \u003cli\u003eDetails sample preparation methods for ion chromatography\u003c\/li\u003e \u003cli\u003eDiscusses hyphenated methods IC-MS and IC-ICP-MS used in determining both the total element contents and its elements\u003c\/li\u003e \u003cli\u003eDetails speciation analysis used in studying biochemical cycles of selected chemical compounds; determining toxicity and ecotoxicity of elements; food and pharmaceuticals quality control; and in technological process control and clinical analytics\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003eList of Contributors ix\u003c\/p\u003e \u003cp\u003ePreface xi\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1 Principles and Applications of Ion Chromatography 1\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eRajmund Michalski\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e1.1 Principles of Ion Chromatography, 1\u003c\/p\u003e \u003cp\u003e1.1.1 Introduction, 1\u003c\/p\u003e \u003cp\u003e1.1.2 Stationary Phases, 6\u003c\/p\u003e \u003cp\u003e1.1.3 Eluents, 13\u003c\/p\u003e \u003cp\u003e1.1.4 Suppressors, 16\u003c\/p\u003e \u003cp\u003e1.1.5 Detection Methods, 18\u003c\/p\u003e \u003cp\u003e1.2 Ion Chromatography Applications, 23\u003c\/p\u003e \u003cp\u003e1.2.1 Speciation Analysis with the Hyphenated Methods of IC-ICP-MS and IC-MS, 29\u003c\/p\u003e \u003cp\u003e1.3 Sample Preparation for Ion Chromatography, 32\u003c\/p\u003e \u003cp\u003e1.4 Selected Methodological Aspects of Ion Determination with Ion Chromatography, 34\u003c\/p\u003e \u003cp\u003e1.5 Ion Chromatography Development Perspectives, 37\u003c\/p\u003e \u003cp\u003e1.6 References, 37\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2 Mass Spectrometric Detectors for Environmental Studies 47\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eMaria Balcerzak\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e2.1 Introduction, 47\u003c\/p\u003e \u003cp\u003e2.2 Mass Spectrometric Detectors, 49\u003c\/p\u003e \u003cp\u003e2.2.1 Ionization Methods, 50\u003c\/p\u003e \u003cp\u003e2.2.2 Mass Analyzers, 58\u003c\/p\u003e \u003cp\u003eAcknowledgments, 62\u003c\/p\u003e \u003cp\u003e2.3 References, 62\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3 High-Performance Liquid Chromatography Coupled to Inductively Coupled Plasma MS\/Electrospray Ionization MS 79\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eJürgen Mattusch\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e3.1 Separation Principles, 79\u003c\/p\u003e \u003cp\u003e3.1.1 Ion Chromatography (Anion\/Cation Exchange, Mixed Mode), 80\u003c\/p\u003e \u003cp\u003e3.1.2 High-Performance Liquid Chromatography (Reversed-Phase Mode, HILIC), 81\u003c\/p\u003e \u003cp\u003e3.1.3 Size Exclusion Chromatography (SEC) (Gel Filtration Chromatography, GFC), 82\u003c\/p\u003e \u003cp\u003e3.2 Detection Principles, 83\u003c\/p\u003e \u003cp\u003e3.2.1 Common Detection in IC: Conductivity, UV–Vis, Electrochemical Detection, 83\u003c\/p\u003e \u003cp\u003e3.2.2 Element Specific Detection, 83\u003c\/p\u003e \u003cp\u003e3.3 Hyphenated Techniques, 87\u003c\/p\u003e \u003cp\u003e3.3.1 HPLC(IC)–ICP-MS, 87\u003c\/p\u003e \u003cp\u003e3.4 HPLC(IC)–ICP-MS\/ESI-MS, 90\u003c\/p\u003e \u003cp\u003e3.4.1 Fundamentals, 90\u003c\/p\u003e \u003cp\u003e3.4.2 Methodology of Data Evaluation, 90\u003c\/p\u003e \u003cp\u003e3.4.3 Technical Requirements, 91\u003c\/p\u003e \u003cp\u003e3.5 Applications and Conclusion, 91\u003c\/p\u003e \u003cp\u003e3.6 References, 102\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4 Application of IC-MS in Organic Environmental Geochemistry 109\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eKlaus Fischer\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e4.1 Introduction, 109\u003c\/p\u003e \u003cp\u003e4.2 Carboxylic Acids, 114\u003c\/p\u003e \u003cp\u003e4.2.1 Molecular Structure, Molecular Interaction Potential, and Chromatographic Retention, 114\u003c\/p\u003e \u003cp\u003e4.2.2 Environmental Analysis of Carboxylic Acids by Ion Exclusion Chromatography–Mass Spectrometry (HPICE-MS), 116\u003c\/p\u003e \u003cp\u003e4.2.3 Environmental Analysis of Carboxylic Acids by Ion-Exchange Chromatography–Mass Spectrometry (HPI-EC-MS), 124\u003c\/p\u003e \u003cp\u003e4.3 Carbohydrates, 135\u003c\/p\u003e \u003cp\u003e4.3.1 Structural Diversity and Ion Chromatographic Behavior, 135\u003c\/p\u003e \u003cp\u003e4.3.2 Environmental Analysis of Carbohydrates by Various IC-MS Methods, 136\u003c\/p\u003e \u003cp\u003e4.4 Amines and Amino Acids, 143\u003c\/p\u003e \u003cp\u003e4.5 Trends and Perspectives, 144\u003c\/p\u003e \u003cp\u003e4.6 References, 145\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5 Analysis of Oxyhalides and Haloacetic Acids in Drinking Water Using IC-MS and IC-ICP-MS 152\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eKoji Kosaka\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e5.1 Introduction, 152\u003c\/p\u003e \u003cp\u003e5.2 Source of Oxyhalides and HAAs, 154\u003c\/p\u003e \u003cp\u003e5.3 Analysis of Oxyhalides and HAAs, 158\u003c\/p\u003e \u003cp\u003e5.3.1 Suppressed IC-MS, 158\u003c\/p\u003e \u003cp\u003e5.3.2 Nonsuppressed IC-MS and LC-MS, 162\u003c\/p\u003e \u003cp\u003e5.3.3 IC-ICP-MS, 165\u003c\/p\u003e \u003cp\u003e5.4 Application for Monitoring of Oxyhalides and HAAs in Drinking Water, 166\u003c\/p\u003e \u003cp\u003e5.4.1 Oxyhalides, 166\u003c\/p\u003e \u003cp\u003e5.4.2 HAAs, 171\u003c\/p\u003e \u003cp\u003eSummary, 171\u003c\/p\u003e \u003cp\u003e5.5 References, 172\u003c\/p\u003e \u003cp\u003e\u003cb\u003e6 Analysis of Various Anionic Metabolites in Plant and Animal Material by IC-MS 178\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eAdam Konrad Jagielski and Michal Usarek\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e6.1 Introduction, 178\u003c\/p\u003e \u003cp\u003e6.2 Optimization of HPIC and Ms Settings, 179\u003c\/p\u003e \u003cp\u003e6.2.1 HPIC Settings, 179\u003c\/p\u003e \u003cp\u003e6.2.2 MS Settings, 183\u003c\/p\u003e \u003cp\u003e6.2.3 HPIC-MS Settings, 185\u003c\/p\u003e \u003cp\u003e6.2.4 Extraction of Metabolites from Cells and Tissues, 189\u003c\/p\u003e \u003cp\u003e6.3 Application of the Method in Analysis of Metabolites in Plant and Animal Material, 191\u003c\/p\u003e \u003cp\u003e6.3.1 Analysis of Metabolites from Cell Cultures (Primary Cultures as well as Established Cell Lines), 192\u003c\/p\u003e \u003cp\u003e6.3.2 Analysis of Metabolites from Solid Tissues, 192\u003c\/p\u003e \u003cp\u003e6.3.3 Extraction of Metabolites from Plants, 194\u003c\/p\u003e \u003cp\u003e6.4 Conclusions, 196\u003c\/p\u003e \u003cp\u003e6.5 References, 197\u003c\/p\u003e \u003cp\u003e\u003cb\u003e7 Analysis of Perchlorate Ion in Various Matrices Using Ion Chromatography Hyphenated with Mass Spectrometry 199\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eJay Gandhi\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e7.1 Introduction, 199\u003c\/p\u003e \u003cp\u003e7.2 Precautions Unique to Ion Chromatography–Mass Spectrometry, 200\u003c\/p\u003e \u003cp\u003e7.2.1 Instrumental and Operating Parameters, 201\u003c\/p\u003e \u003cp\u003e7.3 Results and Discussion, 204\u003c\/p\u003e \u003cp\u003eAcknowledgment, 209\u003c\/p\u003e \u003cp\u003e7.4 References, 209\u003c\/p\u003e \u003cp\u003e\u003cb\u003e8 Sample Preparation Techniques for Ion Chromatography 210\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eWolfgang Frenzel and Rajmund Michalski\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e8.1 Introduction, 210\u003c\/p\u003e \u003cp\u003e8.2 When and Why is Sample Preparation Required in Ion Chromatography? 213\u003c\/p\u003e \u003cp\u003e8.3 Automation of Sample Preparation (IN-LINE Techniques), 215\u003c\/p\u003e \u003cp\u003e8.4 Sample Preparation Methods, 217\u003c\/p\u003e \u003cp\u003e8.4.1 Filtration and Ultrafiltration, 219\u003c\/p\u003e \u003cp\u003e8.4.2 Solid-Phase Extraction (SPE), 220\u003c\/p\u003e \u003cp\u003e8.4.3 Liquid–Liquid Extraction, 225\u003c\/p\u003e \u003cp\u003e8.4.4 Gas-Phase Separations, 226\u003c\/p\u003e \u003cp\u003e8.4.5 Precipitation, 226\u003c\/p\u003e \u003cp\u003e8.4.6 Membrane-Based Separations and Sample Treatment, 227\u003c\/p\u003e \u003cp\u003e8.5 Trace Analysis and Preconcentration for Ion Chromatographic Analysis, 238\u003c\/p\u003e \u003cp\u003e8.5.1 Preconcentration Using SPE, 239\u003c\/p\u003e \u003cp\u003e8.5.2 Membrane-Based In-Line Preconcentration, 241\u003c\/p\u003e \u003cp\u003e8.6 In-Line Preseparations Using Two-Dimensional Ion Chromatography (2D-IC), 243\u003c\/p\u003e \u003cp\u003e8.7 Sample Preparation of Solid Samples, 244\u003c\/p\u003e \u003cp\u003e8.7.1 Dissolution and Aqueous or Acid Extraction, 246\u003c\/p\u003e \u003cp\u003e8.7.2 Wet-Chemical Acid Digestions, 247\u003c\/p\u003e \u003cp\u003e8.7.3 UV Photolytic Digestion, 248\u003c\/p\u003e \u003cp\u003e8.7.4 Fusion Methods, 249\u003c\/p\u003e \u003cp\u003e8.7.5 Dry Ashing and Combustion Methods, 249\u003c\/p\u003e \u003cp\u003e8.8 Air Analysis Using Ion Chromatography – Application to Gases and Particulate Matter, 251\u003c\/p\u003e \u003cp\u003e8.9 Postcolumn Eluent Treatment Prior to Ms Detection, 255\u003c\/p\u003e \u003cp\u003e8.10 Concluding Remarks, 257\u003c\/p\u003e \u003cp\u003e8.11 References, 258\u003c\/p\u003e \u003cp\u003eIndex 267\u003c\/p\u003e \u003cb\u003eRajmund Michalski\u003c\/b\u003e works at the Institute of Environmental Engineering of Polish Academy of Sciences. He has authored\/edited a dozen of books and over 250 publications about applications of ion chromatography in environmental samples analysis, as well as application of modern analytical methods and techniques for environmental protection and assessment. Since 2005 he has annually organized the since international ion chromatography conference in Poland. \u003cp\u003e\u003cb\u003eIntroduces the reader to the field of ion chromatography, species analysis and hyphenated methods  including the theory and practice of several analytical methods\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eIn recent years, the importance of monitoring and controlling environmental pollutants has become apparent in all parts of the world. As a result, analysts have increased their efforts to identify and determine toxic substances in air, water, wastewaters, food, and other sectors of our environment. Ion chromatography has been used in most areas of analytical chemistry and has become a versatile and powerful technique for the analysis of a vast number of inorganic and organic ions present in samples.\u003c\/p\u003e \u003cp\u003eThe coupling of ion chromatography with multi-dimensional detectors such as mass spectrometer (MS) or an inductively coupled plasma mass spectrometer (ICP-MS), known as the hyphenated methods, can achieve outstanding sensitivities and selectivities. \u003ci\u003eApplication of IC-MS and IC-ICP-MS in Environmental Research\u003c\/i\u003e introduces the reader to the field of ion chromatography, species analysis and hyphenated methods. These hyphenated methods provide valuable information for unambiguous peak identification. While IC–ICP-MS is used for element-specific analysis, IC–MS allows the identification of parent compounds and corresponding metabolites. \u003cbr\u003e\u003cbr\u003eWritten by leading experts in the field \u003ci\u003eApplication of IC-MS and IC-ICP-MS in Environmental Research\u003c\/i\u003e features:\u003c\/p\u003e \u003cul\u003e \u003cli\u003ePrinciples and applications of ion chromatography\u003c\/li\u003e \u003cli\u003eMass spectrometric detectors for environmental studies\u003c\/li\u003e \u003cli\u003eHigh performance liquid chromatography coupled to inductively coupled plasma MS\/electrospray ionization MS\u003c\/li\u003e \u003cli\u003eApplication of IC-MS in organic environmental geochemistry\u003c\/li\u003e \u003cli\u003eAnalysis of oxyhalides and haloacetic acids in drinking water using IC-MS\u003c\/li\u003e \u003cli\u003eand IC-ICP-MS\u003c\/li\u003e \u003cli\u003eAnalysis of various anionic metabolites in plant and animal material by IC-MS\u003c\/li\u003e \u003cli\u003eAnalysis of perchlorate ion in various matrices using ion chromatography hyphenated with mass spectrometry\u003c\/li\u003e \u003cli\u003eSample preparation methods for ion chromatography\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003eAlthough speciation analysis by using hyphenated methods such as IC-MS and IC-ICP-MS is relatively expensive, it is gaining more and more importance. This method is used to deal with situations that require both determination of total element contents and consideration for various forms in which these elements occur. Employees of laboratories analyzing environmental samples and carried out species analysis will find this book a valuable resource in identifying and determining toxic substances in air, water, wastewaters, food, and other sectors of our environment.\u003c\/p\u003e \u003cp\u003e\u003cb\u003eRajmund Michalski\u003c\/b\u003e works at the Institute of Environmental Engineering of Polish Academy of Sciences. He has authored\/edited a dozen of books and over 250 publications about applications of ion chromatography in environmental samples analysis, as well as application of modern analytical methods and techniques for environmental protection and assessment. Since 2005 he has annually organized the since international ion chromatography conference in Poland.\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e","brand":"Wiley","offers":[{"title":"Default Title","offer_id":47988747763941,"sku":"NP9781118862001","price":139.95,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9781118862001.jpg?v=1761781432","url":"https:\/\/k12savings.com\/products\/application-of-ic-ms-and-ic-icp-ms-in-environmental-research-isbn-9781118862001","provider":"K12savings","version":"1.0","type":"link"}