The Analytical Chemistry Laboratory Companion

The Analytical Chemistry Laboratory Companion is essential for both students and professionals, as it provides quick, clear explanations on critical topics in analytical chemistry, equipping you with the statistical tools necessary to ensure accurate and reliable data interpretation.

The Analytical Chemistry Laboratory Companion serves as a reference guide for students and professionals alike who need quick explanations on specific topics, laboratory operations, the structure of designing experiments, and the use of statistics to gain increased accuracy, precision, repeatability, and reproducibility of data. This volume will also provide in-depth and advanced studies and build the necessary background knowledge for success in the field.

This companion provides a concise examination of the various analytical tools used for chemistry, and defines basic analytical instrument principles, techniques, and applications in addition to exploring statistical tools useful in data interpretation, test result reporting, and common root causes for faulty data with suggested remedies. The introduction provides a concise guide on foundational topics such as developing standard operating procedures, laboratory safety, instrumental analytical methods, and common statistical tools useful for data interpretation. This companion covers both wet chemical and instrumental analysis, including their principles, applications, and pitfalls. The Analytical Chemistry Laboratory Companion is a must-have, comprehensive guide in the field of analytical chemistry.

Preface xxv

Acknowledgement xxvii

Introduction 1

Part 1: Wet Chemistry 93

Titration 95

Gravimetric Methods 123

Precipitation Methods 141

Extraction Methods 151

Digestion Methods 171

Colorimetric Methods 181

Part 2: Instrumental Analysis 191

Spectroscopy 193

Chromatography 273

Part 3: Thermal Analysis 449

Dynamic Thermal Mechanical Analysis (DTMA) and Thermal Mechanical Analysis (TMA) 451

Appendix 501

Quality 551

General Accounting for the Laboratory 589

Review of Chemical Synthesis 667

References and Review 783

Index 787

Michael D. Holloway is President of 5th Order Industry, which provides competency development and training. He has over 38 years of industry and holds 16 professional certifications. His publications include eight authored books, numerous contributions to other books, and a patent. He is an expert in failure analysis, reliability engineering, and designed experiments for science and engineering.

The Analytical Chemistry Laboratory Companion is essential for both students and professionals, as it provides quick, clear explanations on critical topics in analytical chemistry, equipping you with the statistical tools necessary to ensure accurate and reliable data interpretation.

The Analytical Chemistry Laboratory Companion serves as a reference guide for students and professionals alike who need quick explanations on specific topics, laboratory operations, the structure of designing experiments, and the use of statistics to gain increased accuracy, precision, repeatability, and reproducibility of data. This volume will also provide in-depth and advanced studies and build the necessary background knowledge for success in the field.

This companion provides a concise examination of the various analytical tools used for chemistry, and defines basic analytical instrument principles, techniques, and applications in addition to exploring statistical tools useful in data interpretation, test result reporting, and common root causes for faulty data with suggested remedies. The introduction provides a concise guide on foundational topics such as developing standard operating procedures, laboratory safety, instrumental analytical methods, and common statistical tools useful for data interpretation. This companion covers both wet chemical and instrumental analysis, including their principles, applications, and pitfalls. The Analytical Chemistry Laboratory Companion is a must-have, comprehensive guide in the field of analytical chemistry.