{"product_id":"synthesis-and-technique-in-inorganic-chemistry-isbn-9780935702484","title":"Synthesis and Technique in Inorganic Chemistry","description":"This well-known laboratory manual introduces students to modern synthetic and instrumental techniques currently used in inorganic chemistry.\u003cbr\u003ePreviously by Angelici, this laboratory manual for an upper-level undergraduate or graduate course in inorganic synthesis has for many years been the standard in the field. In this newly revised “third edition,” the manual has been extensively updated to reflect new developments in inorganic chemistry. Twenty-three experiments are divided into five sections: solid state chemistry, main group chemistry, coordination chemistry, organometallic chemistry, and bioinorganic chemistry. The included experiments are safe, have been thoroughly tested to ensure reproducibility, are illustrative of modern issues in inorganic chemistry, and are capable of being performed in one or two laboratory periods of three or four hours. Because facilities vary from school to school, the authors have included a broad range of experiments to help provide a meaningful course in almost any academic setting. Each clearly written \u0026amp; illustrated experiment begins with an introduction that highlights the theme of the experiment, often including a discussion of a particular characterization method that will be used, followed by the experimental procedure, a set of problems, a listing of suggested Independent Studies, and literature references.Introduction\u003cbr\u003eSafety\u003cbr\u003eLaboratory Procedures\u003cbr\u003eResearch Notebook\u003cbr\u003eStandard References\u003cbr\u003ePart I. Solid State Chemistry\u003cbr\u003eExperiment 1--High-Temperature Synthesis of the Superconductor YBa2Cu3O7Tube Furnace Preparation\u003cbr\u003eSuperconductivity\u003cbr\u003eIodometric Titrations\u003cbr\u003eExperiment 2--The Layered Solids VOPO4(H2O)2 and VO(HPO4)(H2O)0.5Powder X-Ray Diffraction\u003cbr\u003eOxidation of Alcohols to Ketones\u003cbr\u003eExperiment 3--The Molecular Sieve Zeolite-XSol-gel Synthesis\u003cbr\u003eHigh Pressure Synthesis\u003cbr\u003eIon Exchange in Microporous Solids\u003cbr\u003ePart II. Main Group Chemistry\u003cbr\u003eExperiment 4--The Borane-Amine Adduct BH3NH2C(CH3)3Lewis Acids and Bases\u003cbr\u003eExperiment 5--Buckminsterfullerene, C60, and Its ElectrochemistrySoxhlet Extraction\u003cbr\u003eCyclic Voltammetry\u003cbr\u003eExperiment 6--Vacuum-Line Synthesis of GeH4Vacuum Line and Trap-to-Trap Purification\u003cbr\u003eVapor Pressure and Molecular Weight Determination of a Volatile Compound\u003cbr\u003eGas Phase IR Spectroscopy\u003cbr\u003eExperiment 7--Tin Chemistry: Coordination Complexes and Organometallic DerivativesNMR Spectroscopy\u003cbr\u003eLinkage Isomerism\u003cbr\u003eExperiment 8--Synthesis of (C6H5)2PCH2CH2P(C6H5)2 in Liquid Ammonia\u003cbr\u003eSynthesis in Liquid Ammonia\u003cbr\u003eExperiment 9--Electrolytic Synthesis of K2S2O8Electrolytic Preparation\u003cbr\u003ePart III. Coordination Chemistry\u003cbr\u003eExperiment 10--Ion Exchange Separation of Chromium Complexes\u003cbr\u003eIon Exchange Chromatography\u003cbr\u003eExperiment 11--Metal-Metal Quadruple Bonds\u003cbr\u003eMolecular Orbital Theory\u003cbr\u003eExperiment 12--The Magnetic Susceptibility of Mn(acac)3Magnetism of Transition Metal Complexes\u003cbr\u003eThe Gouy Method\u003cbr\u003eThe Evans MethodsExperiment 13--Cobalt Ammines and their Ligand Substitution KineticsConductivity of Ionic Complexes\u003cbr\u003eKinetics of Aquation of [Co(NH3)5Cl]2+\u003cbr\u003eExperiment 14--Optical Resolution of Co(en)33+Separation of Diastereomers by Crystallization\u003cbr\u003eOptical Rotations\u003cbr\u003eSuction Filtration\u003cbr\u003eExperiment 15--Metal Dithiolenes and the Use of Quaternary Ammonium Salts\u003cbr\u003eQuaternary Ammonium Salts\u003cbr\u003ePart IV. Organometallic Chemistry\u003cbr\u003eExperiment 16--The Metal-Arene Complex [1,3,5-C6H3(CH3)3]Mo(CO)3IR Spectra of Metal Carbonyls\u003cbr\u003eExperiment 17--Organo-iron Chemistry: (C5H5)2Fe2(CO)4 and (C5H5)Fe(CO)2(CH3)Schlenk Line Synthesis\u003cbr\u003eInfrared Spectra of Solutions\u003cbr\u003eExperiment 18--The Metal Carbonyl Cluster Fe3(CO)12Mass Spectrometry\u003cbr\u003eExperiment 19--Microscale Synthesis of Vaska's Complex\u003cbr\u003eMicroscale Synthesis\u003cbr\u003eSolid State IR Spectra\u003cbr\u003eExperiment 20--The Air-Sensitive Sandwich Complex Nickelocene\u003cbr\u003eGlove Bag Manipulations\u003cbr\u003eSublimation\u003cbr\u003ePart V. Bioinorganic Chemistry\u003cbr\u003eExperiment 21--Cobaloximes: Models of Vitamin-B12 Coenzymes\u003cbr\u003eEnzyme Models\u003cbr\u003eExperiment 22--Amino Acid Complexes: Stability Constants of Ni(glycinate)n(2 - n)+Amino Acid ChemistrypH TitrationspKa and Successive Stability Constant Determination\u003cbr\u003eExperiment 23--Bioinorganic Coordination Chemistry: Copper (II) Tetraphenylporphyrinate\u003cbr\u003ePorphyrin Chemistry\u003cbr\u003eThin-Layer Chromatography\u003cbr\u003eColumn Chromatography\u003cbr\u003eNotes to the Instructor\u003cbr\u003eAppendices\u003cbr\u003eNMR and Mass Spectra\u003cbr\u003eIndex\"Each experiment is well chosen and collectively they present a sufficiently broad spectrum of synthesis and compound characterization techniques to provide an excellent education for any student who completes them…The writing style is clear and concise and at a level that advanced undergraduate students can clearly comprehend. It is highly recommended as a textbook for a one-semester advanced inorganic synthesis course.\" --Synth. React. Inorg. Met.-Org. Chem., 30(3), 569-570 (2000) \u003cbr\u003e\u003cbr\u003e\"This is an excellent update to a classic inorganic chemistry laboratory text. One of the strengths of this book is that there is something here for everyone. The experiments described in the third edition illustrate a wide variety of topics in inorganic chemistry ranging from classic coordination chemistry to more recent advances in the fields of organometallic, solid state, and bioinorganic chemistry.\" --Professor Margret J. Geselbracht, Reed College","brand":"University Science Books","offers":[{"title":"Default Title","offer_id":48233601106149,"sku":"NP9780935702484","price":94.0,"currency_code":"USD","in_stock":false}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/1842\/7735\/files\/9780935702484.jpg?v=1767737701","url":"https:\/\/k12savings.com\/es\/products\/synthesis-and-technique-in-inorganic-chemistry-isbn-9780935702484","provider":"K12savings","version":"1.0","type":"link"}