{"product_id":"fundamentals-of-environmental-sampling-and-analysis-2e-set-isbn-9781394244621","title":"Fundamentals of Environmental Sampling and Analysis, 2e Set","description":"\u003cp\u003eThis book introduces a comprehensive overview on the fundamentals and applications of environmental sampling and analysis for students in environmental science and engineering as well as environmental professionals involved in sampling and analytical work.\u003c\/p\u003e \u003cp\u003eThe book details fundamentals of sampling, selection of standard methods, QA\/QC, sample preparation, chemical and instrumental principles, and method applications to various contaminants in environmental matrices (air, water, soil, waste, and biological samples). The book gives an integrated introduction to sampling and analysis – both are essential to quality environmental data. For example, contrary to other books that introduce a specific area of sampling and analysis, this text provides a balanced mix of field sampling and laboratory analysis, essential knowledge in chemistry\/statistics\/hydrology\/regulations, wet chemical methods for conventional chemicals as well as various modern instrumental techniques for contaminants of emerging concerns. The new edition adds three standalone chapters regarding the basics of analytical and organic chemistry, environmental data analysis, mass spectrometry and other significant amounts of new materials such as time-integrated passive sampling, incremental sampling, green sample preparation, Raman spectroscopy, chiral separation, and non-target analysis. In addition, the second edition provides more examples, visual aids, case studies, and end-of-chapter exercise problems to enhance a better understanding of the fundamentals of environmental sampling and analysis while incorporating current literature (mostly peer-reviewed journal papers) regarding the applications and challenges in the field of environmental sampling and analysis.\u003c\/p\u003e \u003cp\u003e\u003cb\u003eFundamentals of Environmental Sampling and Analysis, 2nd Edition TOC:\u003c\/b\u003e\u003cbr\u003e\u003cbr\u003eList of Case Studies xiii\u003c\/p\u003e \u003cp\u003eList of Boxes xiv\u003c\/p\u003e \u003cp\u003ePreface xvi\u003c\/p\u003e \u003cp\u003eNew in the Second Edition xviii\u003c\/p\u003e \u003cp\u003eAbout the Author xxi\u003c\/p\u003e \u003cp\u003eWhom This Book Is Written For xxii\u003c\/p\u003e \u003cp\u003eTo the Instructor xxiii\u003c\/p\u003e \u003cp\u003eAcknowledgments xxiv\u003c\/p\u003e \u003cp\u003eList of Symbols xxvi\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1 Introduction to Environmental Data Acquisition 1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e1.1 Introduction 2\u003c\/p\u003e \u003cp\u003e1.2 Environmental Sampling 9\u003c\/p\u003e \u003cp\u003e1.3 Environmental Analysis 9\u003c\/p\u003e \u003cp\u003eChapter Themes 13\u003c\/p\u003e \u003cp\u003eReferences 13\u003c\/p\u003e \u003cp\u003eQuestions 14\u003c\/p\u003e \u003cp\u003eProblems 15\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2 Basics of Analytical and Organic Chemistry 16\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e2.1 Basic Concepts from Analytical Chemistry 17\u003c\/p\u003e \u003cp\u003e2.2 Basic Concepts from Organic Chemistry 27\u003c\/p\u003e \u003cp\u003eChapter Themes 47\u003c\/p\u003e \u003cp\u003eReferences 48\u003c\/p\u003e \u003cp\u003eQuestions 49\u003c\/p\u003e \u003cp\u003eProblems 51\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3 Basics of Environmental Data Validation and Analysis 55\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e3.1 Measurements of Central Tendency and Dispersion 56\u003c\/p\u003e \u003cp\u003e3.2 Understanding Probability Distributions 59\u003c\/p\u003e \u003cp\u003e3.3 Hypothesis Testing and Type I and II Errors 65\u003c\/p\u003e \u003cp\u003e3.4 Detection of Outliers 67\u003c\/p\u003e \u003cp\u003e3.5 Analysis of Censored Data 72\u003c\/p\u003e \u003cp\u003e3.6 Analysis of Spatial and Time Series Data 77\u003c\/p\u003e \u003cp\u003eChapter Themes 80\u003c\/p\u003e \u003cp\u003eReferences 81\u003c\/p\u003e \u003cp\u003eQuestions 82\u003c\/p\u003e \u003cp\u003eProblems 83\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4 Environmental Sampling Design 87\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e4.1 Planning and Sampling Protocols 88\u003c\/p\u003e \u003cp\u003e4.2 Sampling Environmental Population 91\u003c\/p\u003e \u003cp\u003e4.3 Environmental Sampling Approaches: Where and When 95\u003c\/p\u003e \u003cp\u003e4.4 Estimating Sample Numbers and Sampling Frequencies 108\u003c\/p\u003e \u003cp\u003eChapter Themes 112\u003c\/p\u003e \u003cp\u003eReferences 113\u003c\/p\u003e \u003cp\u003eQuestions 115\u003c\/p\u003e \u003cp\u003eProblems 116\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5 Environmental Sampling Techniques 120\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e5.1 General Guidelines of Environmental Sampling Techniques 121\u003c\/p\u003e \u003cp\u003e5.2 Grab Sampling Techniques for Various Media: Practical Approaches and Tips 136\u003c\/p\u003e \u003cp\u003e5.3 Time-Integrated Sampling and Sensing Techniques 148\u003c\/p\u003e \u003cp\u003eChapter Themes 153\u003c\/p\u003e \u003cp\u003eReferences 154\u003c\/p\u003e \u003cp\u003eQuestions 156\u003c\/p\u003e \u003cp\u003eProblems 158\u003c\/p\u003e \u003cp\u003e\u003cb\u003e6 Methodology and Quality Assurance\/Quality Control of Environmental Analysis 159\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e6.1 Overview on Standard Methodologies 160\u003c\/p\u003e \u003cp\u003e6.2 Selection of Standard Methods 169\u003c\/p\u003e \u003cp\u003e6.3 Field Quality Assurance\/Quality Control 175\u003c\/p\u003e \u003cp\u003e6.4 Analytical Quality Assurance\/Quality Control 177\u003c\/p\u003e \u003cp\u003eChapter Themes 185\u003c\/p\u003e \u003cp\u003eReferences 186\u003c\/p\u003e \u003cp\u003eQuestions 187\u003c\/p\u003e \u003cp\u003eProblems 189\u003c\/p\u003e \u003cp\u003e\u003cb\u003e7 Wet Chemical and Field Methods for Common Environmental Parameters 191\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e7.1 Basic Operations in Environmental Laboratories 192\u003c\/p\u003e \u003cp\u003e7.2 Wet Chemical Methods and Common Techniques in Environmental Analysis 200\u003c\/p\u003e \u003cp\u003e7.3 Analytical Principles for Common Wet Chemical Methods 204\u003c\/p\u003e \u003cp\u003e7.4 Field Monitoring Testing Kits and Sensors 221\u003c\/p\u003e \u003cp\u003eChapter Themes 224\u003c\/p\u003e \u003cp\u003eReferences 224\u003c\/p\u003e \u003cp\u003eQuestions 225\u003c\/p\u003e \u003cp\u003eProblems 226\u003c\/p\u003e \u003cp\u003e\u003cb\u003e8 Fundamentals of Sample Preparation for Environmental Analysis 229\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e8.1 Overview of Sample Preparation 230\u003c\/p\u003e \u003cp\u003e8.2 Sample Preparation for Metal Analysis 233\u003c\/p\u003e \u003cp\u003e8.3 Extraction for SVOC and Non-VOC from Liquid or Solid Samples 240\u003c\/p\u003e \u003cp\u003e8.4 Sample Preparation for VOC in Liquid and Solid Samples 251\u003c\/p\u003e \u003cp\u003e8.5 Post-Extraction Cleanup of Organic Compounds 255\u003c\/p\u003e \u003cp\u003e8.6 Derivatization for GC and HPLC Analysis 257\u003c\/p\u003e \u003cp\u003eChapter Themes 260\u003c\/p\u003e \u003cp\u003eReferences 260\u003c\/p\u003e \u003cp\u003eQuestions 262\u003c\/p\u003e \u003cp\u003eProblems 263\u003c\/p\u003e \u003cp\u003e\u003cb\u003e9 Molecular Spectroscopic Methods in Environmental Analysis 264\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e9.1 An Introduction to Molecular Spectroscopy 265\u003c\/p\u003e \u003cp\u003e9.2 UV-Visible Spectroscopy 271\u003c\/p\u003e \u003cp\u003e9.3 Infrared Spectroscopy 286\u003c\/p\u003e \u003cp\u003e9.4 Raman Spectrometry 296\u003c\/p\u003e \u003cp\u003e9.5 Photoluminescence and Chemiluminescence 299\u003c\/p\u003e \u003cp\u003eChapter Themes 300\u003c\/p\u003e \u003cp\u003eReferences 301\u003c\/p\u003e \u003cp\u003eQuestions 302\u003c\/p\u003e \u003cp\u003eProblems 305\u003c\/p\u003e \u003cp\u003e\u003cb\u003e10 Atomic Spectroscopy for Metal Analysis 306\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e10.1 Introduction to the Principles of Atomic Spectroscopy 307\u003c\/p\u003e \u003cp\u003e10.2 Instruments for Atomic Spectroscopy 313\u003c\/p\u003e \u003cp\u003e10.3 Selection of the Proper Atomic Spectroscopic Techniques 320\u003c\/p\u003e \u003cp\u003e10.4 Speciation of Metals in Environmental Samples 325\u003c\/p\u003e \u003cp\u003e10.5 Practical Tips to Metal Analysis 326\u003c\/p\u003e \u003cp\u003eChapter Themes 331\u003c\/p\u003e \u003cp\u003eReferences 332\u003c\/p\u003e \u003cp\u003eQuestions 333\u003c\/p\u003e \u003cp\u003eProblems 335\u003c\/p\u003e \u003cp\u003e\u003cb\u003e11 Chromatographic Methods for Environmental Analysis 336\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e11.1 Introduction to Chromatography 337\u003c\/p\u003e \u003cp\u003e11.2 Instruments of Chromatographic Methods 356\u003c\/p\u003e \u003cp\u003e11.3 Common Detectors for Chromatography 363\u003c\/p\u003e \u003cp\u003e11.4 Applications of Chromatographic Methods in Environmental Analysis 371\u003c\/p\u003e \u003cp\u003e11.5 Practical Tips to Chromatographic Methods 375\u003c\/p\u003e \u003cp\u003eChapter Themes 379\u003c\/p\u003e \u003cp\u003eReferences 380\u003c\/p\u003e \u003cp\u003eQuestions 381\u003c\/p\u003e \u003cp\u003eProblems 383\u003c\/p\u003e \u003cp\u003e\u003cb\u003e12 Electrochemical Methods for Environmental Analysis 385\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e12.1 Introduction to Electrochemical Theories 386\u003c\/p\u003e \u003cp\u003e12.2 Potentiometric Applications in Environmental Analysis 395\u003c\/p\u003e \u003cp\u003e12.3 Voltammetric Applications in Environmental Analysis 401\u003c\/p\u003e \u003cp\u003eChapter Themes 406\u003c\/p\u003e \u003cp\u003eReferences 407\u003c\/p\u003e \u003cp\u003eQuestions 408\u003c\/p\u003e \u003cp\u003eProblems 410\u003c\/p\u003e \u003cp\u003e\u003cb\u003e13 Mass Spectrometry in Environmental Analysis 411\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e13.1 Basics of Mass Spectrometry 412\u003c\/p\u003e \u003cp\u003e13.2 Ionization Techniques 417\u003c\/p\u003e \u003cp\u003e13.3 Mass Analyzers 428\u003c\/p\u003e \u003cp\u003e13.4 Hyphenated Mass Spectrometric Methods 435\u003c\/p\u003e \u003cp\u003e13.5 Mass Spectra and Molecule Fragmentation 442\u003c\/p\u003e \u003cp\u003e13.6 Mass Spectrometric Applications in Environmental Analysis 448\u003c\/p\u003e \u003cp\u003eChapter Themes 451\u003c\/p\u003e \u003cp\u003eReferences 452\u003c\/p\u003e \u003cp\u003eQuestions 453\u003c\/p\u003e \u003cp\u003eProblems 458\u003c\/p\u003e \u003cp\u003e\u003cb\u003e14 Other Instrumental Methods in Environmental Analysis 459\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e14.1 Nuclear Magnetic Resonance (NMR) Spectroscopy 460\u003c\/p\u003e \u003cp\u003e14.2 Surface and Microscopic Characterization 474\u003c\/p\u003e \u003cp\u003e14.3 Radiochemical Analysis 484\u003c\/p\u003e \u003cp\u003e14.4 Screening Methods Using Immunoassay 489\u003c\/p\u003e \u003cp\u003eChapter Themes 489\u003c\/p\u003e \u003cp\u003eReferences 490\u003c\/p\u003e \u003cp\u003eQuestions 491\u003c\/p\u003e \u003cp\u003eProblems 494\u003c\/p\u003e \u003cp\u003eAppendix A: Common Abbreviations and Acronyms 495\u003c\/p\u003e \u003cp\u003eAppendix B1: National Primary Drinking Water Regulations 503\u003c\/p\u003e \u003cp\u003eAppendix B2: National Ambient Air Quality Standards 507\u003c\/p\u003e \u003cp\u003eAppendix C: Structures and Properties of Important Organic Pollutants 508\u003c\/p\u003e \u003cp\u003eAppendix D1: Standard Normal Cumulative Probabilities 519\u003c\/p\u003e \u003cp\u003eAppendix D2: Percentiles of Student’s t Distribution 521\u003c\/p\u003e \u003cp\u003eAppendix D3: Critical Values for the F-Distribution 523\u003c\/p\u003e \u003cp\u003eAppendix E: Required Containers, Preservation Techniques, and Holding Times 526\u003c\/p\u003e \u003cp\u003eAppendix F: Answers to Selected Questions and Problems 529\u003c\/p\u003e \u003cp\u003eAppendix G: Periodic Table 537\u003c\/p\u003e \u003cp\u003eIndex 538\u003c\/p\u003e \u003cp\u003e\u003cb\u003eFundamentals of Environmental Sampling and Analysis, 2nd Edition Solutions Manual TOC:\u003c\/b\u003e\u003cbr\u003e\u003cbr\u003eChapter 1 Questions 1\u003c\/p\u003e \u003cp\u003eProblems 5\u003c\/p\u003e \u003cp\u003eChapter 2 Questions 6\u003c\/p\u003e \u003cp\u003eProblems 12\u003c\/p\u003e \u003cp\u003eChapter 3 Questions 17\u003c\/p\u003e \u003cp\u003eProblems 19\u003c\/p\u003e \u003cp\u003eChapter 4 Questions 33\u003c\/p\u003e \u003cp\u003eProblems 39\u003c\/p\u003e \u003cp\u003eChapter 5 Questions 49\u003c\/p\u003e \u003cp\u003eProblems 53\u003c\/p\u003e \u003cp\u003eChapter 6 Questions 56\u003c\/p\u003e \u003cp\u003eProblems 63\u003c\/p\u003e \u003cp\u003eChapter 7 Questions 67\u003c\/p\u003e \u003cp\u003eProblems 74\u003c\/p\u003e \u003cp\u003eChapter 8 Questions 79\u003c\/p\u003e \u003cp\u003eProblems 87\u003c\/p\u003e \u003cp\u003eChapter 9 Questions 90\u003c\/p\u003e \u003cp\u003eProblems 96\u003c\/p\u003e \u003cp\u003eChapter 10 Questions 100\u003c\/p\u003e \u003cp\u003eProblems 108\u003c\/p\u003e \u003cp\u003eChapter 11 Questions 110\u003c\/p\u003e \u003cp\u003eProblems 121\u003c\/p\u003e \u003cp\u003eChapter 12 Questions 124\u003c\/p\u003e \u003cp\u003eProblems 131\u003c\/p\u003e \u003cp\u003eChapter 13 Questions 133\u003c\/p\u003e \u003cp\u003eProblems 145\u003c\/p\u003e \u003cp\u003eChapter 14 Questions 147\u003c\/p\u003e \u003cp\u003eProblems 160\u003c\/p\u003e 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